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Preparation of In-Situ Synthesized SiC Particles Reinforced Highly Porous Si_3N_4 Ceramics by Gel-casting

机译:凝胶浇铸法原位合成SiC颗粒增强高多孔Si_3N_4陶瓷

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摘要

In this paper, highly porous Si_3N_4 ceramics with high strength, homogeneous microstructure were fabricated by introducing a proper amount of nanometer carbon in the Si_3N_4 slurry by gel-casting. Scanning electron microscopy, X-ray diffraction, Archimedes water-displacement method and three-point bending tests were employed to analyze the microstructures and mechanical properties of the sintered bodies. It was shown by the XRD analysis that SiC particles were formed in the sintered bodies. The pillar β- Si_3N_4 morphology, homogeneous microstructure and the SiC particles as a reinforcement phase are the contributing factors for high porosity and good mechanical behavior.
机译:本文通过凝胶浇铸在Si_3N_4浆料中引入适量的纳米碳,从而制备了具有高强度,均匀组织的高孔隙率Si_3N_4陶瓷。采用扫描电子显微镜,X射线衍射,阿基米德水置换法和三点弯曲试验对烧结体的组织和力学性能进行了分析。 XRD分析表明,在烧结体中形成了SiC颗粒。支柱β-Si_3N_4的形貌,均匀的微观结构和SiC颗粒作为增强相是导致高孔隙率和良好机械性能的因素。

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