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Galcium Phosphate Coatings Produced by Ion Beam Sputtering/Mixing Deposition: Their Manufacture, Structure and In Vitro Properties

机译:离子束溅射/混合沉积法制备磷酸镓钙涂层的制备,结构和体外性能

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Ion beam sputtering/mixing deposition was used to produce dense and homogeneous calcium phosphate (Ca-P) coatings on titanium substrate. The mixing beam was either Ar~+ or N~+ ions. Scanning electron microscopy revealed that the deposited coatings had a uniform and dense structure. The calcium to phosphorous ration of these coatings varied between 2.0 to 3.0. It was found that as-deposited coatings were amorphous. Results obtained from Fourier transform infrared spectroscopy (FTIR) showed the existence of the phosphate group in coatings but no distinct absorption band of the hydroxyl group was observed. Compared. Compared with Ca-P coatings produced by Ar~+ beam mixing, Ca-P coatings produced by N~+ beam mixing exhibited a higher dissolution rate in the physiological saline solution and caused a lower proliferation rate of osteoblast cells.
机译:离子束溅射/混合沉积用于在钛基板上生产致密且均匀的磷酸钙(Ca-P)涂层。混合束为Ar〜+或N〜+离子。扫描电子显微镜显示沉积的涂层具有均匀且致密的结构。这些涂层的钙磷比率在2.0至3.0之间变化。发现沉积态的涂层是无定形的。从傅立叶变换红外光谱法(FTIR)获得的结果表明涂层中存在磷酸根,但是没有观察到明显的羟基吸收带。比较。与通过Ar〜+束混合制备的Ca-P涂层相比,通过N〜+束混合制备的Ca-P涂层在生理盐溶液中的溶解速率更高,而成骨细胞的增殖速率更低。

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