Synthesis and characterization of single crystalline PbO nanorods via a facile hydrothermal method

Baoping Jia; Lian Gao

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Synthesis and characterization of single crystalline PbO nanorods via a facile hydrothermal method

机译：简便水热法合成PbO单晶纳米棒及其表征

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Single crystalline β-PbO nanorods with diameter range from 40 to 120 nm and length up to 500 nm have been synthesized via a facile hydrothermal method in the presence of citrate. X-ray diffraction (XRD), transmission electron microscopy (TEM), high-resolution transmission electro-microscope (HRTEM) and SAED were used to characterize the as-obtained samples. An interesting intermediate state of self-assembled β-PbO rod-like nanoparticles was found and the possible formation mechanism of single crystalline β-PbO nanorods was also discussed.

机译：在柠檬酸盐存在下，通过简便的水热法合成了直径为40-120 nm，长度最大为500 nm的单晶β-PbO纳米棒。 X射线衍射（XRD），透射电子显微镜（TEM），高分辨率透射电子显微镜（HRTEM）和SAED用于表征所获得的样品。发现了有趣的自组装β-PbO棒状纳米颗粒的中间状态，并讨论了单晶β-PbO纳米棒的可能形成机理。

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来源
《Materials Chemistry and Physics》 |2006年第3期|p.351-354|共4页
作者
Baoping Jia; Lian Gao;
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作者单位

State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, PR China;

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收录信息美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
原文格式 PDF
正文语种 eng
中图分类工程材料学;工程基础科学;
关键词
inorganic compounds; nanostructure; chemical synthesis; microstructure;

机译：无机化合物;纳米结构;化学合成;微观结构;

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Synthesis and characterization of single crystalline PbO nanorods via a facile hydrothermal method

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