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Mechanical properties of electrodeposited amorphous/crystalline multilayer structures in the Fe-P system

机译:Fe-P体系中电沉积非晶/晶体多层结构的机械性能

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Amorphous/crystalline multilayer structures of Fe-P alloys were deposited electrochemically using the single bath technique. Hall-Petch behavior of microhardness with respect to sublayer thickness was observed down to a sublayer thickness of 15nm. For thinner sublayers, a hardness plateau was obtained. The transition at a sublayer thickness of 15nm coincides with the loss of the multilayer structure as observed in transmission electron microscopy. The transition is a possible result of a change in the amorphous to crystalline sublayer thickness ratio and the interface roughness development during the deposition process. Additionally, crack deflection at the interfaces was observed for the layered structures with small sublayer thickness in microbending experiments.
机译:Fe-P合金的非晶/晶体多层结构使用单浴技术电化学沉积。观察到相对于子层厚度的显微硬度的Hall-Petch行为,直至子层厚度为15nm。对于较薄的子层,获得了硬度平台。在透射电子显微镜下观察到,亚层厚度为15nm时的过渡与多层结构的损失相吻合。该转变是在沉积过程中非晶与结晶子层厚度之比变化和界面粗糙度发展的可能结果。另外,在微弯曲实验中观察到亚层厚度小的层状结构在界面处的裂纹偏转。

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