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Effect of Li addition on the plastic deformation behaviour of AZ31 magnesium alloy

机译:锂的添加对AZ31镁合金塑性变形行为的影响

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The enhancement in the workability, if any, of a dilute Mg alloy, AZ31, with the Li addition is investigated by examining the hot deformation behaviour of AZ31 alloyed with 1, 3 and 5 wt% Li. Compression tests were conducted in the temperature, T, range of 150-400 ℃ and strain rates, ε, ranging from 10~(-3) to 10~(+2) s~(-1). Experimental results show that the deformation behaviour can be divided into three T regimes. In the low T regime (150-200 ℃), an increase in the Li content in AZ31 decreases the twin density with a concomitant enhancement in the non-basal or cross-slip activity. While high Li alloys exhibit low flow stress at low ε in this regime, an increase in ε increases strain hardening rate and twinning activity. Flow localization and shear band formation were observed in most of the alloys in this regime. Deformation in the intermediate T regime (250-300 ℃) leads to dynamic recovery (DRY) at low ε and dynamic re-crystallization (DRX) at high ε, which are the softening mechanisms in Li containing alloys. In high T regime (350-400 ℃), these alloys exhibit softening mechanisms similar to intermediate T regime but high Li alloys surprisingly exhibit higher flow stresses, which is attributed to the higher amount of Li in the solid solution, a result of the dissolution of Li containing precipitates. Non-basal slip and twinning at high ε occur uniformly with homogeneous DRX. A low activation energy for deformation of high Li alloys indicates that the Friedel-Escaig (F-E) mechanism as the rate controlling deformation mechanism. The onset of twinning was examined by the appearance of first local maxima before peak strain in (d~2σ/dε~2) vs. ε curves. Mechanisms responsible for the dependence of critical stress for the onset of DRX on T and ε are also discussed.
机译:通过检查掺有1、3和5 wt%Li的AZ31的热变形行为,研究了添加Li的稀Mg合金AZ31的可加工性的提高。在150-400℃的温度T和10〜(-3)到10〜(+2)s〜(-1)的应变率ε下进行压缩测试。实验结果表明,变形行为可分为三个T型态。在低T态(150-200℃)下,AZ31中Li含量的增加会降低孪晶密度,并同时增强非基层或横向滑移活性。虽然高Li合金在这种情况下在低ε时表现出较低的流应力,但ε的增加会提高应变硬化速率和孪晶活性。在这种状态下,大多数合金中都观察到了流动局部化和剪切带形成。中间T态(250-300℃)的变形导致低ε下的动态回复(DRY)和高ε下的动态再结晶(DRX),这是含锂合金的软化机理。在高T态(350-400℃)下,这些合金表现出类似于中间T态的软化机理,但高Li合金出人意料地表现出更高的流动应力,这归因于固溶体中较高的Li含量,这是溶解的结果。含锂的沉淀。非基面滑动和高ε孪生与均质DRX均匀发生。高Li合金变形的低活化能表明,Friedel-Escaig(F-E)机制是控制速率的变形机制。通过在(d〜2σ/dε〜2)-ε曲线中的峰值应变之前出现的第一个局部最大值来检查孪生的发生。还讨论了引起DRX的临界应力依赖于T和ε的机制。

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