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Exceptional crystal strain hardening determined over macro- to micro- to nano-size scales in continuous spherical indentation tests

机译:在连续球形压痕试验中通过宏观至微达纳米尺寸的卓越晶体应变硬化

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摘要

Calculations of an order of magnitude greater strain hardening coefficient over compression or tensile test measurements are demonstrated for continuous indentation hardness measurements past "pop-in". Analyses were performed at small indentation strains for a macro-ball test on a NaCl crystal and at larger strains measured for rounded points of micro- and nano-tipped indenters in tests of MgO and copper crystal surfaces. The exceptional strain hardening is attributed to the smaller spacing and consequent interactions of the plastically-induced dislocations, including for MgO, the formation of nano-scale sessile dislocations accompanying the imposed three-dimensional deformation. The dislocation-based hardening is much greater than the smaller so-called "Indentation Size Effect (ISE)" of softening obtained at larger, constant strain, penetration depths with Berkovich-type indenters. Such ISE softening is attributed rather to the reverse effect of increasingly larger dislocation separations accompanying the greater plastic indentation depths.
机译:对压缩或拉伸试验测量的数量级阶数大的数量级的计算用于过去“POP-IN”的连续压痕硬度测量。在NaCl晶体上的宏观球试验的小压痕菌株中进行分析,并在MgO和铜晶体表面的测试中测量的微型和纳米尖头压痕的圆形菌株。卓越的应变硬化归因于塑性诱导的脱位的间距较小和随后的相互作用,包括MgO,伴随着施加的三维变形的纳米尺度无梗塞脱臼的形成。基于错位的硬化远大于在较大,恒定的菌株,伯克维奇型压头处获得的软化的较小所谓的“压痕尺寸效应(ISE)”。这种ise软化是归因于伴随着更大的塑料压痕深度的越来越大的位错分离的逆向效果。

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