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Synthesis of (2D) MNPs nanosheets of nickel ferrite using a low-cost co- precipitation process

机译:使用低成本共沉淀法合成镍铁氧体的(2D)MNPs纳米片

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摘要

Herein a low-cost and low temperature co-precipitation process for the preparation of two-dimensional (2D) MNPs nanosheets of nickel ferrite was reported. The influence of the heat treatment on structural, morphological and magnetic properties of 2D MNPs nanosheets of NiFe2O4was investigated. Rietveld analysis was used to confirm the presence of NiFe2O4as of a main phase which corresponding to be the NiFe2O4which crystallizes in cubic spinel type structure withFd3¯mspace group. The average crystallite size (D) and lattice strain (ε) were estimated using the Scherrer’s relation and Williamson-Hall method. The formation of two-dimensional (2D) nanosheets like morphology was observed by SEM images. At room temperature, the saturation magnetization and coercivity of the hard obtained sample were evaluated at room temperature and were found to be 46.9 emu.g−1and 1.14 kOe respectively.
机译:本文报道了低成本和低温共沉淀法制备镍铁氧体二维(2D)MNPs纳米片的方法。研究了热处理对NiFe2O4二维MNPs纳米片结构,形貌和磁性的影响。用Rietveld分析法确认了主相NiFe2O4的存在,该相对应于以Fed3mspace基团的立方尖晶石型结构结晶的NiFe2O4。平均晶粒尺寸(D)和晶格应变(ε)使用Scherrer关系和Williamson-Hall方法估算。通过SEM图像观察到二维(2D)纳米片的形态,如形态。在室温下,对获得的硬质样品在室温下的饱和磁化强度和矫顽力进行了评估,结果分别为46.9μgg-1和1.14kOe。

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