New form of iron orthovanadate FeVO_4·1.5H_2O prepared at normal pressure and low temperature

Khaled Melghit; Abdullah S. Al-Mungi

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New form of iron orthovanadate FeVO_4·1.5H_2O prepared at normal pressure and low temperature

机译：常压低温制备的新形式原钒酸铁FeVO_4·1.5H_2O

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A new form of iron(Ⅲ) orthovanadate(Ⅴ) FeVO_4·1.5H_2O was prepared at low temperature from mixing a boiling solution of iron nitrate with boiling solution of vanadium oxide (obtained by reacting V_2O_5 with few mL of 30 vol.% H_2O_2 following by a dilution with distilled water). The mixture was maintained under stirring for several days at 85℃ in order the product reaches crystallinity. When iron nitrate solution was not heated and added to boiling vanadium oxide solution, it leads to FeVO_4 · 1.1H_2O phase similar to the fervanite mineral.

机译：通过将硝酸铁的沸腾溶液与氧化钒的沸腾溶液混合（通过使V_2O_5与少量的30％（体积）的H_2O_2反应而获得），在低温下制备了一种新形式的原钒酸铁（Ⅴ）FeVO_4·1.5H_2O用蒸馏水稀释）。将混合物在85℃下搅拌几天，以使产物结晶。当不加热硝酸铁溶液并将其添加到沸腾的氧化钒溶液中时，会生成类似于铁锰矿矿物的FeVO_4·1.1H_2O相。

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来源
《Materials Science and Engineering. B, Solid-State Materials for Advanced Technology》 |2007年第3期|p.177-181|共5页
作者
Khaled Melghit; Abdullah S. Al-Mungi;
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作者单位

Chemistry Department, College of Science, P.O. Box 36, Al Khodh 123, Sultane Qaboos University, Oman;

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原文格式 PDF
正文语种 eng
中图分类工程材料学;
关键词
chemical preparation; X-ray methods; iron orthovanadate FeVO_4;

机译：化学制备;X射线法;原钒酸铁FeVO_4;

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New form of iron orthovanadate FeVO_4·1.5H_2O prepared at normal pressure and low temperature

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