• 主题
高级搜索  >
历史搜索 清空历史
首页> 外文期刊>Materials Science and Engineering. B, Solid-State Materials for Advanced Technology >Effects of heat treatment on structural evolution and morphology of powder synthesized by the sol-gel method
【24h】

Effects of heat treatment on structural evolution and morphology of powder synthesized by the sol-gel method

机译：热处理对溶胶-凝胶法合成粉末结构演变和形貌的影响

获取原文
获取原文并翻译 | 示例
           
页面导航
  • 摘要
  • 著录项
  • 相似文献
  • 相关主题

摘要

BaTi_5O_(11) powder was successfully prepared and characterized by the sol-gel method. The mechanisms of BaTi_5O_(11) formation were studied by the fourier transform infrared spectroscopy (FTIR). The IR absorption peaks confirm the existence of a substitution reaction with the chelating reagent corresponding to different modes of vibration characteristic of the acetate group. The X-ray diffraction (XRD) results showed that the formation of single-phase monoclinic BaTi_5O_(11) began at 700℃ and were stable up to 1100℃ in air. The particle sizes observed from scanning electron microscopy (SEM) are about 100 nm for a calcination temperature at 700℃ and 600 nm at 1100℃.
机译：成功制备了BaTi_5O_（11）粉末，并通过溶胶-凝胶法对其进行了表征。通过傅里叶变换红外光谱（FTIR）研究了BaTi_5O_（11）的形成机理。 IR吸收峰证实了与螯合剂的取代反应的存在，其对应于乙酸酯基团的不同振动模式。 X射线衍射（XRD）结果表明，单相单斜BaTi_5O_（11）的形成始于700℃，在空气中最高可稳定到1100℃。对于700℃下的煅烧温度，从扫描电子显微镜（SEM）观察到的粒径为约100nm，而在1100℃下为600nm。

著录项

相似文献

  • 外文文献
  • 中文文献
  • 专利
获取原文

客服邮箱：kefu@zhangqiaokeyan.com

京公网安备：11010802029741号 ICP备案号：京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有

  • 客服微信

  • 服务号