Sextuple ratiometric thermometry based on 980-nm-upconverted green fluorescence of Er~(3+) ions in submicron crystals

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Sextuple ratiometric thermometry based on 980-nm-upconverted green fluorescence of Er~(3+) ions in submicron crystals

机译：基于亚微米晶体中Er〜（3+）离子的980nm上转换绿色荧光的六倍体比重测温法

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980-nm-upconverted 530 and 550 nm Er3+ green fluorescence spectra of Er3+/Yb3+-codoped NaGd(WO4)(2) submicron crystals were measured in the temperature range of 298-383 K. A sextuple ratiometric thermometry is proposed. It is established on the basis of six schemes of fluorescence intensity ratio (FIR) that considers three component peaks of the 530 nm emission band and two component peaks of the 550 nm emission band, which involve electronic transitions between two Stark sublevels of Er3+. The study shows that the phosphor shows strong green fluorescence, which is verified by measured quantum yield, and thermally stable spectral structure desired for the sextuple ratiometric thermometry. All of the six FIR schemes display highly efficient sensing performances with slightly different thermal sensitivities. Each scheme gives a temperature value and the six schemes give an averaged result. In parallel, we have also carried out an ex vivo experimental study on the temperature characteristics of the green fluorescence of the phosphor. Almost same results have been obtained, verifying biological applicability of the phosphor. The ex vivo experimental results also show that the sextuple thermometry increases considerably the accuracy and reliability of temperature measurement in comparison with the conventional intensity integration method.

机译：在298-383 K的温度范围内，测量了Er3 + / Yb3 +掺杂的NaGd（WO4）（2）亚微米晶体的980nm上转换的530 nm和550nm的Er3 +绿色荧光光谱。提出了六元比率的测温法。它是基于六种荧光强度比（FIR）方案建立的，该方案考虑了530 nm发射带的三个组分峰和550 nm发射带的两个组分峰，这涉及Er3 +的两个Stark子级之间的电子跃迁。研究表明，磷光体显示出强烈的绿色荧光，这已通过测得的量子产率得到证实，并且具有六元比率测温法所需的热稳定光谱结构。六个FIR方案中的所有方案均显示出高效的感测性能，而热敏度略有不同。每个方案给出一个温度值，六个方案给出一个平均值。同时，我们还对荧光粉的绿色荧光的温度特性进行了离体实验研究。已经获得几乎相同的结果，证实了磷光体的生物学适用性。离体实验结果还表明，与常规强度积分法相比，六元体测温法显着提高了温度测量的准确性和可靠性。

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《Materials science & engineering》 |2020年第3期|110512.1-110512.9|共9页
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Tianjin Univ Minist Educ Sch Precis Instruments & Oproelect Engn Dept Optoelect & Informat Engn Tianjin 300072 Peoples R China|Tianjin Univ Minist Educ Key Lab Oproelect Informat Technol Tianjin 300072 Peoples R China;

Tianjin Sino German Univ Appl Sci 2 Yanshan Rd Haihe Educ Pk Tianjin 300350 Peoples R China;

Univ Paris VI Pierre & Marie Curie Univ Dept Engn 4 Pl Jussieu F-75005 Paris France;

City Univ Hong Kong Dept Elect Engn Hong Kong Peoples R China;

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Sensors; Sextuple ratiometric thermometry; Green fluorescence; Er3+/Yb3+-codoped submicron crystals; Ex vivo measurement;

机译：传感器;六元比率测温法;绿色荧光;Er3 + / Yb3 +掺杂的亚微米晶体;离体测量;

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1. Sextuple ratiometric thermometry based on 980-nm-upconverted green fluorescence of Er3+ ions in submicron crystals [J] . Liu Mei-Hong, Wang Xiao, Xu Qing, Materials science & engineering, C. Materials for Biogical applications . 2020,第期

机译：基于980-nm-uperverded绿色荧光的亚微米晶体中的980-nm-uperverted绿色荧光
2. Er~(3+)-doped BaTiO_(3) nanocrystals for thermometry: Influence of nanoenvironment on the sensitivity of a fluorescence based temperature sensor [J] . Marcio A. R. C. Alencar, Glauco S. Maciel, Cid B. de Araujo, Applied Physics Letters . 2004,第23期

机译：掺Er〜（3+）的BaTiO_（3）纳米晶体的测温：纳米环境对基于荧光的温度传感器灵敏度的影响
3. Optical thermometry through green and red upconversion emissions in Er~(3+)/Yb~(3+)/Li~(+):ZrO_(2) nanocrystals [J] . Lu Liu, Yuxiao Wang, Xueru Zhang, Optics Communications: A Journal Devoted to the Rapid Publication of Short Contributions in the Field of Optics and Interaction of Light with Matter . 2011,第7期

机译：Er〜（3 +）/ Yb〜（3 +）/ Li〜（+）：ZrO_（2）纳米晶体中绿色和红色上转换发射的光学测温
4. Highly sensitive optical thermometry based on the upconversion fluorescence from Yb~(3+)/Er~(3+) codoped La_2(WO_4)_3:Yb~(3+) ,Er~(3+) phosphor [C] . Yan-min Yang, Chao Mi International conference on optical instruments and technology . 2013

机译：基于Yb〜（3 +）/ Er〜（3+）共掺杂La_2（WO_4）_3：Yb〜（3+），Er〜（3+）荧光粉上转换荧光的高灵敏光学测温
5. Optical spectroscopy, crystal field analysis, upconversion and energy transfer studies of Er(3+) doped yttrium vanadate single crystals. [D] . Kabro, Pierre. 1997

机译：掺Er（3+）钒酸钇钇单晶的光谱，晶体场分析，上转换和能量转移研究。
6. A Fusion-Spliced Near-Field Optical Fiber Probe Using Photonic Crystal Fiber for Nanoscale Thermometry Based on Fluorescence-Lifetime Measurement of Quantum Dots [O] . Takuro Fujii, Yoshihiro Taguchi, Toshiharu Saiki, 2011

机译：基于量子点荧光寿命测量的光子晶体光纤熔融拼接近场纳米探针。
7. Vacuum-Ultraviolet and Ultraviolet Fluorescence and Absorption Studies of Er(3+)-Doped Liluf4 Single-Crystals [O] . Sarantopoulou, Evangelia, Kollia, Zoe, Cefalas, Alciviadis Constantinos, 2008

机译：掺Er（3+）的Liluf4单晶的真空紫外和紫外荧光及吸收研究
8. Fluorescence and Excitation Spectra of Bk exp 3+ , CF exp 3+ , and es exp 3+ Ions in Single Crystals of Lacl sub 3 [R] . Hessler, J. P., Caird, J. A., Carnall, W. T., 1977

机译：Lacl sub 3单晶中Bk exp 3 +，CF exp 3+和es exp 3+离子的荧光和激发光谱

Sextuple ratiometric thermometry based on 980-nm-upconverted green fluorescence of Er~(3+) ions in submicron crystals

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