Aminolysis of polyethylene terephthalate surface along with in situ synthesis and stabilizing ZnO nanoparticles using triethanolamine optimized with response surface methodology

Hajar Poortavasoly; Majid Montazer; Tina Harifi

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Aminolysis of polyethylene terephthalate surface along with in situ synthesis and stabilizing ZnO nanoparticles using triethanolamine optimized with response surface methodology

机译：使用响应表面法优化的三乙醇胺对聚对苯二甲酸乙二酯表面进行氨解以及原位合成和稳定ZnO纳米颗粒

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This research concerned the simultaneous polyester surface modification and synthesis of zinc oxide nano-reactors to develop durable photo-bio-active fabric with variable hydrophobicity/hydrophilicity under sunlight For this purpose, triethanolamine (TEA) was applied as a stabilizer and pH adjusting chemical for the aminolysis of polyester surface and enhancing the surface reactivity along with synthesis and deposition of ZnO nanoparticles on the fabric Therefore, TEA played a crucial role in providing the alkaline condition for the preparation of zinc oxide nanoparticles and acting as stabilizer controlling the size of the prepared nanoparticles. The stain-photodegradability regarded as self-cleaning efficiency, wettability and weight change under the process was optimized based on zinc acetate and TEA concentrations, using central composite design (CCD). Findings also suggested the potential of the prepared fabric in inhibiting Staphylococcus aureus and Escherichia coti bacteria growth with greater than 99.99% antibacterial efficiency. Besides, the proposed treatment had no detrimental effect on tensile strength and hand feeling of the polyester fabric.

机译：这项研究涉及同时聚酯表面改性和氧化锌纳米反应器的合成，以开发在阳光下具有可变疏水性/亲水性的耐用光生物活性织物。为此，将三乙醇胺（TEA）用作稳定剂和pH调节化学品用于因此，TEA在为制备氧化锌纳米颗粒提供碱性条件以及控制所制备的大小的稳定剂方面起着至关重要的作用。纳米粒子。使用中央复合设计（CCD），根据乙酸锌和TEA的浓度，优化了该过程中被认为具有自清洁效率，润湿性和重量变化的污渍光降解性。研究结果还表明，所制备的织物具有抑制金黄色葡萄球菌和大肠杆菌的生长潜力，其抗菌效率大于99.99％。此外，所提出的处理对聚酯织物的拉伸强度和手感没有不利影响。

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来源
《Materials science & engineering》 |2016年第1期|495-503|共9页
作者
Hajar Poortavasoly; Majid Montazer; Tina Harifi;
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作者单位

Department of Textile Engineering, Amirkabir University of Technology, Functional Fibrous Structures & Environmental Enhancement (FFSEE), Tehran, Iran;

Department of Textile Engineering, Amirkabir University of Technology, Functional Fibrous Structures & Environmental Enhancement (FFSEE), Tehran, Iran;

Department of Textile Engineering, Amirkabir University of Technology, Functional Fibrous Structures & Environmental Enhancement (FFSEE), Tehran, Iran;

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正文语种 eng
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关键词
Polyester; ZnO nanoparticles; Triethanolamine; Self-cleaning properties; Antibacterial; Central composite design;

机译：聚酯;ZnO纳米颗粒;三乙醇胺自洁性能;抗菌;中央复合设计;

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专利

1. Aminolysis of polyethylene terephthalate surface along with in situ synthesis and stabilizing ZnO nanoparticles using triethanolamine optimized with response surface methodology [J] . Poortavasoly Hajar, Montazer Majid, Harifi Tina Materials science & engineering, C. Materials for Biogical applications . 2016,第Null期

机译：使用响应表面法优化的三乙醇胺对聚对苯二甲酸乙二酯表面进行氨解以及原位合成和稳定ZnO纳米颗粒
2. Optimization of surface treatment for flotation separation of polyvinyl chloride and polyethylene terephthalate waste plastics using response surface methodology [J] . Wang Chongqing, Wang Hui, Liu Younian, Journal of Cleaner Production . 2016,第DECa15期

机译：响应面法优化浮选分离聚氯乙烯和聚对苯二甲酸乙二醇酯废塑料的表面处理
3. In situ synthesis of nano ZnO on starch sized cotton introducing nano photo active fabric optimized with response surface methodology [J] . Khosravian Shokoufeh, Montazer Majid, Malek Reza M. A., Carbohydrate Polymers: Scientific and Technological Aspects of Industrially Important Polysaccharides . 2015,第Null期

机译：在淀粉棉上原位合成纳米ZnO，引入响应面法优化的纳米光敏织物
4. Optimization of Serratia nematodiphila using Response surface methodology to silver nanoparticles synthesis for aquatic pathogen control [C] . S Rajeshkumar, C Malarkodi International Conference on Science, Engineering the Technology . 2018

机译：响应表面方法对水生病原体控制的响应表面方法优化Serratia Nematodiphila
5. Irradiation of polyethylene terephthalate by excimer radiation and surface characterization by contact angle goniometry, infrared spectroscopy and electroosmotic flow [D] . Alagathi Narayanan, Madhusudhan 2009

机译：准分子辐射辐照聚对苯二甲酸乙二醇酯，接触角测角，红外光谱和电渗流表征表面
6. Statistical Optimization of Process Parameters for Lipase-Catalyzed Synthesis of Triethanolamine-Based Esterquats Using Response Surface Methodology in 2-Liter Bioreactor [O] . Hamid Reza Fard Masoumi, Mahiran Basri, Anuar Kassim, 2013

机译：在2升生物反应器中使用响应面法对脂肪酶催化合成三乙醇胺基酯的工艺参数进行统计优化
7. Mycosynthesis of Size-Controlled Silver Nanoparticles through Optimization of Process Variables by Response Surface Methodology [O] . ASMA SHAHZAD, MEHWISH IQTEDAR, HAMID SAEED, 2019

机译：响应面法优化工艺变量优化尺寸控制的银纳米粒子的mycosynesis

Aminolysis of polyethylene terephthalate surface along with in situ synthesis and stabilizing ZnO nanoparticles using triethanolamine optimized with response surface methodology

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