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Detailed chemical analysis of dirt specks in Celgar off-grade pulp

机译:Celgar劣质纸浆中污点的详细化学分析

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Off-grade in Celgar NBSK pulp has been an intermittent problem since 1998. In order to fully understand the cause of the problem, more than 170 dirt specks in Celgar off-grade pulp were collected over a 4 month period starting in 2005. Each individual sample was characterized using preliminary chemical testing. More detailed analytical methods were used on selected samples. This work was able to positively identify slime (biofilm) as the cause of off-grade in more than 70% of the samples examined. Prior to this work, it was not possible to clearly distinguish between slime and pitch during pulp grading at the mill, and off-grade from slime was frequently classified as pitch.rnA simple routine test was implemented to allow graders to clearly distinguish between pitch and slime.rnNitrogen isotope analysis was used to show the source of slime (biofilm) in individual dirt specks. This is the first time that this has been reported in the pulp and paper industry.rnAdditional analytical methods used include SEM/EDS, FTIR-microscope and glycoside composition analysis.
机译:自1998年以来,Celgar NBSK纸浆的不合格问题就一直是一个间歇性的问题。为了全面了解问题的原因,从2005年开始的4个月中,收集了170多个Celgar劣质纸浆的污点。每个人使用初步化学测试对样品进行表征。在选定的样品上使用了更详细的分析方法。这项工作能够在超过70%的受检样品中肯定地识别出粘液(生物膜)是不合格的原因。在进行这项工作之前,不可能在纸浆分级过程中清楚地区分煤泥和沥青,并且通常将煤泥中的劣质煤泥归类为沥青。rn实施了一个简单的常规测试,使分级人员可以清楚地区分煤泥和沥青。氮同位素分析用于显示各个污垢中的煤泥(生物膜)来源。这是纸浆和造纸行业的首次报道。使用的其他分析方法包括SEM / EDS,FTIR显微镜和糖苷成分分析。

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