Nanocrystalline Metals and Oxides II: Reverse Microemulsions

W. Hartl; Ch. Beck; M. Roth

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Nanocrystalline Metals and Oxides II: Reverse Microemulsions

机译：纳米晶体金属和氧化物II：反向微乳液

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In this contribution the synthesis of nanocrystalline metal oxides and the formation of NH_4MnF_3 by microemul- sion techniques is investigated in detail. The size and size distribution of the primary reverse micelles are deter- mined by dynamic light scattering. Further it was possible to characterize intermediate species in the reaction pro- cess The size of the final nanocrystal material was evaluated from the line broadening of X-ray reflections. The size distribution is very narrow and for the metaloxides a strong correlation exists between the size of the final product and the reverse micelles.

机译：在这一贡献中，详细研究了纳米晶体金属氧化物的合成和通过微乳化技术形成NH_4MnF_3。初级反胶束的大小和大小分布由动态光散射确定。进一步可以表征反应过程中的中间物种。最终的纳米晶体材料的尺寸是通过X射线反射的线展宽来评估的。尺寸分布非常窄，对于金属氧化物，最终产品的尺寸和反胶束之间存在很强的相关性。

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《Berichte der Bunsengesellschaft fur Physikalische Chemie》 |1997年第11期|p.1714-1717|共4页
作者
W. Hartl; Ch. Beck; M. Roth;
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正文语种 eng
中图分类化学;
关键词
Light; Scattering; Micelles; Nanocrystalline Materials;

机译：光;散射;胶束;纳米晶材料;

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2. Low-Temperature Reverse Microemulsion Synthesis, Characterization, and Photocatalytic Performance of Nanocrystalline Titanium Dioxide [J] . Zhang Liu, Zicong Jian, Jianzhang Fang, International Journal of Photoenergy . 2012,第Pta2期

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4. Microemulsions composed of metal complex surfactants, bis(octylethylenediamine (= OE)) Zn(II), Cd(II), and Pd(II) chlorides, in water/chloroform and water/benzene systems [C] . Masay asu Iida, Hua Er, Naoko Hisamatsu, International conference on colloid and surface science . 2001

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5. The application of tetrakis(dimethylamino)ethylene chemiluminescence in characterization of the surface properties of metal oxides and reversed microemulsion systems. [D] . Huang, Chien-Chang. 2009

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6. Reverse Microemulsion-mediated Synthesis of Monometallic and Bimetallic Early Transition Metal Carbide and Nitride Nanoparticles [O] . Sean T. Hunt, Yuriy Román-Leshkov 2015

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7. Effect of Metals Oxides Loading on the Modification of Microstructure and Phase Transformation of Nanocrystalline CeZrO2 Synthesized Using Water-in-oil-Microemulsion [O] . Hadi Abdul, Ismail Kamariah Noor, Shah M Nazri Abu 2015

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Nanocrystalline Metals and Oxides II: Reverse Microemulsions

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