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Thermal analysis, statistical predicting, and optimization of the flexural properties of natural fiber biocomposites using Box- Be hn ken experimental design

机译:使用Box-Be hn ken实验设计进行天然纤维生物复合材料的热分析,统计预测和挠曲特性的优化

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The object of this study is to investigate the flexural properties of biocomposites based on polypropylene/kenaf fiber/polypropylene-grafted maleic anhydride (PP/kenaf/PP-g-MA) using the response surface methodology. A three-factor, three-level Box-Behnken design, which is the subset of the response surface methodology, has been applied to present mathematical models as a function of kenaf fiber load, fiber length, and PP-g-MA compatibilizer content for the prediction of flexural strength and modulus behavior of the natural fiber biocomposite. Three levels were chosen for the considered parameters as follows: kenaf fiber (10-30 wt%), fiber length (2-10 mm), and PP-g-MA (1-5 wt%). Optimum compositions for better flexural properties were obtained from contour plots and response surface methodology. The results obtained using the design expert software showed the optimal flexural strength and modulus to be 53.66 and 3442 MPa, respectively. The obtained R-2 values and normal probability plots indicated a good agreement between the experimental results and those predicted by the model. Finally, the morphology and thermal stability of the samples were evaluated by scanning electron microscopy and thermogravimetric analysis.
机译:这项研究的目的是利用响应表面方法研究基于聚丙烯/洋麻纤维/聚丙烯接枝的马来酸酐(PP /洋麻/ PP-g-MA)的生物复合材料的挠曲性能。三因子,三级Box-Behnken设计(是响应面方法的子集)已应用于提出作为洋麻纤维负载,纤维长度和PP-g-MA增容剂含量的函数的数学模型。天然纤维生物复合材料的抗弯强度和模量行为的预测。为考虑的参数选择了以下三个级别:洋麻纤维(10-30 wt%),纤维长度(2-10 mm)和PP-g-MA(1-5 wt%)。从轮廓图和响应面方法获得了最佳的抗弯性能最佳组合物。使用设计专家软件获得的结果显示最佳弯曲强度和模量分别为53.66和3442 MPa。获得的R-2值和正态概率图表明实验结果与模型预测的结果吻合良好。最后,通过扫描电子显微镜和热重分析评估了样品的形态和热稳定性。

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