Note: Sample chamber for in situ x-ray absorption spectroscopy studies of battery materials

Pelliccione C.J.; Timofeeva E.V.; Katsoudas J.P.; Segre C.U.

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Note: Sample chamber for in situ x-ray absorption spectroscopy studies of battery materials

机译：注意：用于电池材料的原位X射线吸收光谱研究的样品室

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In situ x-ray absorption spectroscopy (XAS) provides element-specific characterization of both crystalline and amorphous phases and enables direct correlations between electrochemical performance and structural characteristics of cathode and anode materials. In situ XAS measurements are very demanding to the design of the experimental setup. We have developed a sample chamber that provides electrical connectivity and inert atmosphere for operating electrochemical cells and also accounts for x-ray interactions with the chamber and cell materials. The design of the sample chamber for in situ measurements is presented along with example XAS spectra from anode materials in operating pouch cells at the Zn and Sn K-edges measured in fluorescence and transmission modes, respectively.

机译：原位X射线吸收光谱（XAS）提供了结晶相和非晶相的特定元素表征，并实现了电化学性能与阴极和阳极材料的结构特征之间的直接关联。原位XAS测量对实验装置的设计要求很高。我们已经开发了一个样品室，该样品室为操作电化学电池提供了电连接性和惰性气氛，并且还考虑了与该室和电池材料之间的X射线相互作用。给出了用于原位测量的样品室的设计，以及在荧光和透射模式下分别测量的工作袋单元中Zn和Sn K边缘处阳极袋中阳极材料的示例XAS光谱。

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《Review of Scientific Instruments》 |2014年第12期|1-3|共3页
作者
Pelliccione C.J.; Timofeeva E.V.; Katsoudas J.P.; Segre C.U.;
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Department of Physics and CSRRI, Illinois Institute of Technology, Chicago, Illinois 60616, USA;

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1. Simultaneous in Situ X-ray Absorption Spectroscopy and X-ray Diffraction Studies on Battery Materials: The Case of Fe0.5TiOPO4 [J] . Bleith Peter, van Beek Wouter, Kaiser Hermann, The journal of physical chemistry, C. Nanomaterials and interfaces . 2015,第7期

机译：电池材料同时原位X射线吸收光谱法和X射线衍射研究：Fe0.5TiOPO4的情况
2. In situ Fe K-edge X-ray absorption spectroscopy study during cycling of Li2FeSiO4 and Li2.2Fe0.9SiO4 Li ion battery materials [J] . Brownrigg Alexander W., Mountjoy Gavin, Chadwick Alan V., Journal of Materials Chemistry, A. Materials for energy and sustainability . 2015,第14期

机译：Li2FeSiO4和Li2.2Fe0.9SiO4锂离子电池材料循环过程中原位Fe K边缘X射线吸收光谱研究
3. Potential-Resolved In Situ X-ray Absorption Spectroscopy Study of Sn and SnO2 Nanomaterial Anodes for Lithium-Ion Batteries [J] . Pelliccione Christopher J., Timofeeva Elena V., Segre Carlo U. The journal of physical chemistry, C. Nanomaterials and interfaces . 2016,第10期

机译：锂离子电池Sn和SnO2纳米材料阳极的电位分辨原位X射线吸收光谱研究
4. Reaction Mechanism Analysis of a Li-O_2 Battery: Structure of Electrode/Electrolyte Interface Probed Via Soft X-Ray Absorption Spectroscopy, Hard X-Ray Photoelectron Spectroscopy, and in-Situ Hard X-Ray Diffraction [C] . C. Yogi, K. Kamiguchi, N. Takao, Batteries beyond lithium-ion . 2015

机译：Li-O_2电池的反应机理分析：通过软X射线吸收光谱，硬X射线光电子能谱和原位硬X射线衍射探测的电极/电解质界面结构
5. In situ x-ray absorption spectroscopy study of tin anode nanomaterials for lithium-ion batteries. [D] . Pelliccione, Christopher J. 2015

机译：锂离子电池锡阳极纳米材料的原位X射线吸收光谱研究。
6. Structural Evolution of Ag-LEV Zeolite upon Heating:An In Situ Single-Crystal X-ray Diffraction (SC-XRD) and X-rayAbsorption Spectroscopy (XAS) Study [O] . Georgia Cametti, *, Andreas C. Scheinost, 2020

机译：Ag-lev沸石在加热时的结构演变：一种原位单晶X射线衍射（SC-XRD）和X射线吸收光谱（XAS）研究
7. In situ Fe K-edge X-ray absorption spectroscopy study during cycling of Li2FeSiO4 and Li2.2Fe0.9SiO4 Li ion battery materials [O] . Brownrigg, A.W., Mountjoy, G., Chadwick, A.V., 2015

机译：Li2FeSiO4和Li2.2Fe0.9SiO4锂离子电池材料循环过程中的原位Fe K边缘X射线吸收光谱研究

Note: Sample chamber for in situ x-ray absorption spectroscopy studies of battery materials

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