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首页> 外文期刊>Review of Scientific Instruments >Study of Pressure Calibration and Pressure Distribution in a Piston‐Cylinder High Pressure Press
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Study of Pressure Calibration and Pressure Distribution in a Piston‐Cylinder High Pressure Press

机译:活塞缸高压压力机中压力校准和压力分布的研究

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The pressure loss in a high pressure vessel of a piston‐cylinder press has been studied at the bismuth (I‐II) and (II‐III) transitions. This was accomplished by measuring the abrupt diminution of volume of bismuth, which was surrounded by a solid pressure transmitting medium, at the pressure‐induced phase transitions. The study of pressure loss has been made by measuring three pressure losses which are defined as follows: (1) Pressure loss I is due to the interfacial friction between the cylinder and the piston. (2) Pressure loss II is due to the interfacial friction between the cylinder and the solid pressure transmitting medium which separates the piston and bismuth. (3) Pressure loss III originates within ``the sample‐containing cross section of the cylinder'' and is due to the internal friction of the medium. Experiment showed that the pressure loss III is the largest among the pressure losses. The difference between the true pressure on the bottom of a sample and the average pressure on the top of the piston due to pressure loss III has been formulated. This pressure loss study has been applied to the pressure calibration of a high pressure furnace containing a sample under investigation and also to the drawing of a diagram of pressure distribution in the furnace.
机译:在铋(I-II)和(II-III)过渡处研究了活塞缸压力机的高压容器中的压力损失。这是通过测量在压力引起的相变时铋的体积突然减小而实现的,铋的体积被固体压力传递介质包围。压力损失的研究是通过测量三个压力损失来进行的,它们定义如下:(1)压力损失I是由于气缸和活塞之间的界面摩擦引起的。 (2)压力损失II是由于气缸与将活塞和铋分开的固体压力传递介质之间的界面摩擦引起的。 (3)压力损失III源自``圆柱体的样品横截面''内,是由于介质的内部摩擦引起的。实验表明,压力损失III在压力损失中最大。计算了样品底部的真实压力与由于压力损失III导致的活塞顶部的平均压力之间的差。该压力损失研究已应用于装有待调查样品的高压炉的压力校准,并且还应用于炉中压力分布图的绘制。

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