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Facile synthesis of high silver content MOD ink by using silver oxalate precursor for inkjet printing applications

机译：使用草酸银前驱体轻松合成高银含量的MOD油墨，用于喷墨印刷应用

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摘要

In this paper, a particle-free MOD ink (MOD = metal-organic-decomposition) of high silver content was directly used for inkjet printing silver conductive patterns on PI substrate. The ink was synthesized by using silver oxalate as precursor, ethylamine as a complexing ligand, ethyl alcohol and ethylene glycol as the solvent. The chemical and physical properties of the solution ink were investigated. The MOD ink has 27.6 wt.% of silver. The deposited films on PI substrate were thermally treated at a range of temperatures and times, and then analyzed in terms of their morphology and resistivity. The silver film cured at 170 degrees C for 30 min had a resistivity of 8.4 mu Omega.cm. The printed patterns on PI substrate cured at 150 degrees C for 30 min showed metalized silver with low resistivity (8.6 mu Omega.cm), high reflection, and good adhesion. (C) 2015 Elsevier B.V. All rights reserved.
机译：在本文中，直接将高银含量的无颗粒MOD油墨（MOD =金属有机分解）用于在PI基板上喷墨印刷银导电图案。以草酸银为前驱体，乙胺为配位体，乙醇和乙二醇为溶剂合成油墨。研究了溶液油墨的化学和物理性质。 MOD油墨具有27.6重量％的银。在一定温度和时间范围内对PI基板上的沉积膜进行热处理，然后根据其形态和电阻率进行分析。在170℃下固化30分钟的银膜的电阻率为8.4μΩ·cm。在150℃下固化30分钟的PI基板上的印刷图案显示出金属化的银，其电阻率低（8.6μOΩ.cm），反射率高且附着力好。 （C）2015 Elsevier B.V.保留所有权利。

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  • 来源
    《Thin Solid Films》 |2015年第31期|381-387|共7页
  • 作者

    Dong Yue; Li Xiaodong; Liu Shaohong; Zhu Qi; Li Ji-Guang; Sun Xudong;

  • 作者单位

    Northeastern Univ, Sch Met & Mat, Minist Educ, Key Lab Anisotropy & Texture Mat, Shenyang 110819, Liaoning, Peoples R China;

    Northeastern Univ, Sch Met & Mat, Minist Educ, Key Lab Anisotropy & Texture Mat, Shenyang 110819, Liaoning, Peoples R China;

    Northeastern Univ, Sch Met & Mat, Minist Educ, Key Lab Anisotropy & Texture Mat, Shenyang 110819, Liaoning, Peoples R China;

    Northeastern Univ, Sch Met & Mat, Minist Educ, Key Lab Anisotropy & Texture Mat, Shenyang 110819, Liaoning, Peoples R China;

    Natl Inst Mat Sci, Adv Mat Proc Unit, Tsukuba, Ibaraki 3050044, Japan;

    Northeastern Univ, Sch Met & Mat, Minist Educ, Key Lab Anisotropy & Texture Mat, Shenyang 110819, Liaoning, Peoples R China;

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  • 正文语种 eng
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  • 关键词

    Silver oxalate; Metal organic decomposition inks (MOD inks); Conductive films; Inkjet printing;

    机译：草酸银;金属有机分解油墨（MOD油墨）;导电膜;喷墨印刷;

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