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A study on the microstructure and gas sensing properties of ITO nanocrystals

机译:ITO纳米晶体的微观结构和气敏特性的研究

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摘要

The effect of different SnO_2 loading (0-25 wt.%) on the microstructural, electrical and gas sensing properties of ITO (indium tin oxide) nanocrystals synthesized by a non-aqueous sol-gel technique was evaluated. TEM, HRTEM and XRD characterization has shown that all samples have a uniform grain morphology and narrow particle size distribution, while a remarkable size reduction was observed with the increase of tin loading in the mixed oxide formulation. Redox properties of the samples were also characterized by H_2-TPR. The gas sensing properties of ITO films towards CO (100-1000 ppm) and ethanol (50-400 ppm) have been investigated. On the basis of the characterization data, explanations of the observed sensing behaviour of ITO films are given.
机译:评估了不同的SnO_2负载量(0-25 wt。%)对通过非水溶胶-凝胶技术合成的ITO(铟锡氧化物)纳米晶体的微观结构,电学和气体传感性能的影响。 TEM,HRTEM和XRD表征表明,所有样品均具有均匀的晶粒形态和窄的粒径分布,而随着混合氧化物配方中锡含量的增加,观察到明显的尺寸减小。样品的氧化还原性质也通过H_2-TPR表征。研究了ITO膜对CO(100-1000 ppm)和乙醇(50-400 ppm)的气敏特性。根据表征数据,给出了观察到的ITO膜传感行为的解释。

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