Hydrothermal synthesis and crystal structure of a Novel Pb(II) Coordination polymer

Wang X.-Y.; Ma S.; Li T.; Seik Weng N.

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Hydrothermal synthesis and crystal structure of a Novel Pb(II) Coordination polymer

机译：新型Pb（II）配位聚合物的水热合成和晶体结构

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The novel coordination polymer, [Pb(1,4-chdc)(L)], 1, (1,4-H 2chdc = cyclohexane-1,4-dicarboxylic acid and L = 11-fluoro-dipyrido[3,2-a:2′,3′-c]phenazine), has been synthesized using a hydrothermal method and characterized by elemental analysis, IR spectroscopy and single-crystal X-ray diffraction. Crystal data: C _(26)H_(19)FN_4O_4Pb, triclinic, space group P1, a = 9.074(5), b = 9.499(5), c = 13.853(5) ?, α = 85.640(5), β = 76.127(5), γ = 74.730(5), V = 1118.2(9) ?~3, Z = 2. The 1,4-chdc ligands link the Pb(II) atoms to form a 1D chain structure. The L ligands are attached on both sides of the chains. Further, π-π interactions among neighboring chains lead to a two-dimensional supramolecular layer.

机译：新型配位聚合物[Pb（1,4-chdc）（L）]，1，（1,4-H 2chdc =环己烷-1,4-二羧酸和L = 11-氟-二吡啶基[3,2- a：2'，3'-c]吩嗪），已使用水热法合成，并通过元素分析，红外光谱和单晶X射线衍射进行了表征。晶体数据：C _（26）H_（19）FN_4O_4Pb，三斜晶系，空间群P1，a = 9.074（5），b = 9.499（5），c = 13.853（5）α，α= 85.640（5），β ＝ 76.127（5），γ＝ 74.730（5），V ＝ 1118.2（9）→3，Z ＝ 2。1,4-chdc配体连接Pb（II）原子形成一维链结构。 L配体连接在链的两侧。此外，相邻链之间的π-π相互作用导致二维超分子层。

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《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2011年第1期|共4页
作者
Wang X.-Y.; Ma S.; Li T.; Seik Weng N.;
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正文语种 eng
中图分类化学;
关键词
11-Fluoro-dipyrido3; 2-a 2′; 3′-cphenazine; 4-dicarboxylic Acid; Coordination Polymer; Crystal Structure; Cyclohexane-1;

机译：11-氟二吡啶并[3;2-a 2';3'-c]吩嗪;4-二羧酸;配位聚合物;晶体结构;环己烷-1;

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Hydrothermal synthesis and crystal structure of a Novel Pb(II) Coordination polymer

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