Study on the synthesis of heat-resistant PMMA

Dong Shaosheng; Zhang Zhiqian; Wei Yuezhen

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Study on the synthesis of heat-resistant PMMA

机译：耐热PMMA的合成研究

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摘要

N-cyclohexylmaleimide (CHMI) and styrene (St) were used to copolymerize with methyl methacrylate (MMA) to synthesize heat-resistant poly(methyl methacrylate) (PMMA) by a solution copolymerization method and a suspension copolymerization method. Residual CHMI concentrations in the copolymers were analyzed by gas chromatography. Effects of styrene on residual CHMI concentration, glass transition temperature (Tg), molecular weight, and molecular weight distribution were studied.

机译：使用N-环己基马来酰亚胺（CHMI）和苯乙烯（St）与甲基丙烯酸甲酯（MMA）共聚，通过溶液共聚法和悬浮共聚法合成耐热性聚甲基丙烯酸甲酯（PMMA）。通过气相色谱分析共聚物中残余的CHMI浓度。研究了苯乙烯对残余CHMI浓度，玻璃化转变温度（Tg），分子量和分子量分布的影响。

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来源
《Journal of Applied Polymer Science》 |1999年第10期|共5页
作者
Dong Shaosheng; Zhang Zhiqian; Wei Yuezhen;
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原文格式 PDF
正文语种 eng
中图分类高分子化学（高聚物）;高分子化合物产品;有机化学;
关键词
Polymethyl methacrylates; Synthesis (chemical); Copolymerization; Polyimides; Polystyrenes; Heat resistance; Copolymers; Molecular weight distribution; Glass transition; Thermal effects; Gas chromatography; Polycyclohexylmaleimide; Solution copolymerization; Suspension copolymerization;

机译：聚甲基丙烯酸甲酯;合成（化学）;共聚;聚酰亚胺;聚苯乙烯;耐热性;共聚物;分子量分布;玻璃化转变;热效应;气相色谱;聚环己基马来酰亚胺;溶液共聚;悬浮共聚;

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专利

1. Study on the Synthesis of Heat-Resistant PMMA [J] . SHAOSHENG DONG Journal of Applied Polymer Science . 1999,第9期

机译：耐热PMMA的合成研究
2. Synthesis and self-assembly of PMMA-b-(u)PE-b-PMMA copolymers: study the aggregate morphology in toluene vapor [J] . Qian Jianyong, Ding Linfeng, Zhu Gejiong, Journal of Polymer Research . 2019,第6期

机译：PMMA-B-（U）PE-B-PMMA共聚物的合成和自组装：研究甲苯蒸汽的骨料形态
3. Study of Synthesis and Evaluation of Heat-Resistant Coatings Based on Silicon-Boron Carbide-Zirconium Boride-Aluminum Oxide Composite [J] . Bankovskaya I. B., Nikolaev A. N., Kolovertnov D. V., Glass Physics and Chemistry: A Journal on the Structural, Physical, and Chemical Properties and Nature of Inorganic Glasses and Glass-Forming Melts . 2018,第5期

机译：基于硅 - 硼化碳化硅 - 硼铝氧化铝复合材料的耐热涂层的合成与评价研究
4. Synthesis and initial characterization of PS-PMMA blend film for annealing induced phase mixing study [C] . S. Tripathi, P. N. Rao, S. N. Jha DAE Solid State Physics Symposium . 2019

机译：用于退火诱导相混合研究的PS-PMMA共混膜的合成与初步表征
5. Synthesis of PMMA-b-PEO diblock and PMMA-b-PEO-b-PMMA triblock copolymers and their applications as polymeric surfactants in emulsion polymerization [D] . Wu, Wen-Lin 1991

机译：PMMA-b-PEO二嵌段和PMMA-b-PEO-b-PMMA三嵌段共聚物的合成及其在乳液聚合中作为聚合物表面活性剂的应用
6. Synthesis and Study of the Optical Properties of PMMA Microspheres and Opals [O] . Mayra Matamoros-Ambrocio, Enrique Sánchez-Mora, Estela Gómez-Barojas, 2021

机译：PMMA微球和蛋白石光学性质的合成与研究
7. Synthesis and Conductivity Studies of Poly(Methyl Methacrylate) (PMMA) by Co-Polymerization and Blending with Polyaniline (PANi) [O] . Helyati Abu Hassan Shaari, Muhammad Mahyiddin Ramli, Mohd Nazim Mohtar, 2021

机译：共聚聚合和混合聚苯胺（PANI）聚苯胺（PANI）的合成与导电性研究
8. Fundamental Studies on the Synthesis of Heat-Resistant Polymers [R] . Dalelio, G. F. 1966

机译：耐热聚合物合成的基础研究

Study on the synthesis of heat-resistant PMMA

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