Synthesis and crystal structure of a macrocyclic azidotetraamine copper(II) complex

Choi KY.

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Synthesis and crystal structure of a macrocyclic azidotetraamine copper(II) complex

机译：大环叠氮基四胺铜（II）配合物的合成和晶体结构

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The complex [Cu(L)N-3](H2O)(ClO4) (1) (L = 3,14-dimethyl-2,6,13,17-tetraazatricyclo[14,4,0(1,18) 0(7,12)]docosane) has been prepared and characterized by X-ray crystallography. 1 crystallizes in the monoclinic space group P2(1)/c, with a = 8.907(5), b = 20.036(3), c = 14.773(2) Angstrom, beta = 103.78(2)degrees V = 2560.6(15) Angstrom(3), and Z = 4. The coordination geometry around the Cu(Il) ion is a distorted square-pyramidal with four nitrogen atoms of the macrocycle and one nitrogen atom of the axial azido group. [References: 11]

机译：络合物[Cu（L）N-3]（H2O）（ClO4）（1）（L = 3,14-二甲基-2,6,13,17-四氮杂三环[14,4,0（1,18）0 （7,12）]二十二烷）已制备并通过X射线晶体学表征。 1在单斜空间群P2（1）/ c中结晶，其中a = 8.907（5），b = 20.036（3），c = 14.773（2）埃，β= 103.78（2）度V = 2560.6（15） Ang（3），Z =4。Cu（II）离子周围的配位几何形状是扭曲的方锥，其大环上有四个氮原子，轴向叠氮基上有一个氮原子。 [参考：11]

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《Journal of chemical crystallography》 |1998年第12期|共4页
作者
Choi KY.;
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正文语种 eng
中图分类晶体学;
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Macrocyclic azidotetraamine copper(ii) complex;

机译：大环叠氮基四胺铜（ii）络合物;

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1. Synthesis and crystal structure of a macrocyclic azidotetraamine copper(II) complex [J] . Choi KY. Journal of chemical crystallography . 1998,第12期

机译：大环叠氮基四胺铜（II）配合物的合成和晶体结构
2. Synthesis and properties of a tetraaza macrocyclic ligand containing 2-pyridylmethyl pendant arms and its copper(II) and nickel(II) complexes: crystal structure of the copper(II) complex [J] . Kang SG., Jeong JH., Kim SJ. Polyhedron: The International Journal for Inorganic and Organometallic Chemistry . 1998,第18期

机译：含2-吡啶基甲基侧链的四氮杂大环配体及其铜（II）和镍（II）配合物的合成与性能：铜（II）配合物的晶体结构
3. Synthesis, crystal structure, and magnetic properties of the first nonanuclear lanthanide(III)-copper(II) complexes of macrocyclic oxamide [NaLn(2)Cu(6)] (macrocyclic oxamide=1,4,8,11-tetraazacyclotradecanne-2,3-dione, Ln = Pr, Nd) [J] . Tang JK., Li YZ., Wang QL., Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2002,第8期

机译：大环乙酰胺[NaLn（2）Cu（6）]（大环乙酰胺= 1,4,8,11-四氮杂环戊烷-2）的第一个非核镧系（III）-铜（II）配合物的合成，晶体结构和磁性，3-dione，Ln = Pr，Nd）
4. Synthesis, Crystal structure and antimicrobial activity of a mixed-iigand copper (II) complex Cu(pht)_2 (phen)H_2O [C] . Xi-Lan Hu, Qin Jiang, Xing-You Xu International Conference on Chemical Engineering and Advanced Materials . 2011

机译：混合Iigand铜（II）复合物Cu（PHT）_2（Phen）H_2O的合成，晶体结构和抗微生物活性。
5. I. THE SYNTHESES, SOLUTION BEHAVIOR, CRYSTAL STRUCTURES AND MAGNETIC PROPERTIES OF SOME IMIDAZOLATE BRIDGED COPPER(II) COMPLEXES. II. THE CRYSTAL STRUCTURE AND MAGNETIC PROPERTIES OF A TRICOPPER(II) CLUSTER CONTAINING A TRIPLY BRIDGING CARBONATE GROUP. [D] . KOLKS, GARY ARNOLD. 1980

机译：I.某些咪唑基桥接铜（II）配合物的合成，溶液行为，晶体结构和磁性。二。含碳桥基的三铜（II）簇的晶体结构和磁性。
6. Polymers of ε-Caprolactone Using New Copper(II) and Zinc(II) Complexes as Initiators: Synthesis Characterization and X-Ray Crystal Structures [O] . Andrés F. Posada, Mario A. Macías, Santiago Movilla, 2018

机译：使用新型铜（II）和锌（II）配合物作为引发剂的ε-己内酯聚合物：合成表征和X射线晶体结构
7. Copper complexes with new oxaaza-pendant-armed macrocyclic ligands: X-ray crystal structure of a macrocyclic copper(II) complex [O] . Vicente Manuel, Bastida Rufina, Macías Alejandro, 2005

机译：具有新的oxaaza侧链武装的大环配体的铜配合物：大环铜（II）配合物的X射线晶体结构
8. Crystal and Molecular Structures of a Tricyclic Phosphorus Ester, a Cobalt(III) Macrocyclic Complex and a Trans Coordinated Platinum(II) Compound [R] . Wintergrass, D. J. 1987

机译：三环磷酯，钴（III）大环配合物和反式配位铂（II）化合物的晶体和分子结构

Synthesis and crystal structure of a macrocyclic azidotetraamine copper(II) complex

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