Coupling-Reagent-Free Synthesis of Dipeptides and Tripeptides Using Amino Acid Ionic Liquids

Furukawa Shinya; Fukuyama Takahide; Matsui Akihiro; Kuratsu Mai; Nakaya Ryotaro; Ineyama Takashi; Ueda Hiroshi; Ryu Ilhyong

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Coupling-Reagent-Free Synthesis of Dipeptides and Tripeptides Using Amino Acid Ionic Liquids

机译：使用氨基酸离子液体的无偶联试剂合成二肽和三肽

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A general method for the synthesis of dipeptides has been developed, which does not require any coupling reagents. This method is based on the reaction of readily available HCl salts of amino acid methyl esters with tetrabutylphosphonium amino acid ionic liquids. The isolation procedure of stepwise treatment with AcOH is easy to carry out. The method was extended to the synthesis of tripeptide, tyrosyl-glycyl-glycine, present in IMREG-1, also.

机译：已经开发了合成二肽的通用方法，该方法不需要任何偶联剂。该方法基于容易获得的氨基酸甲酯的HCl盐与四丁基phosph氨基酸离子液体的反应。用AcOH逐步处理的分离过程很容易进行。该方法还扩展到了IMREG-1中也存在的三肽酪氨酸-甘氨酰-甘氨酸的合成。

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《Chemistry: A European journal》 |2015年第34期|共4页
作者
Furukawa Shinya; Fukuyama Takahide; Matsui Akihiro; Kuratsu Mai; Nakaya Ryotaro; Ineyama Takashi; Ueda Hiroshi; Ryu Ilhyong;
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正文语种 eng
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amino acid ionic liquids; coupling-reagent free; dipeptides; tripeptides;

机译：氨基酸离子液体;无偶联剂;二肽;三肽;

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1. Coupling-Reagent-Free Synthesis of Dipeptides and Tripeptides Using Amino Acid Ionic Liquids [J] . Furukawa Shinya, Fukuyama Takahide, Matsui Akihiro, Chemistry: A European journal . 2015,第34期

机译：使用氨基酸离子液体的二肽和三肽无偶联剂合成
2. High Performance Liquid Chromatographic Enantioresolution of Benzoyl Amino Acid, Dipeptides and Tripeptide on #beta#-Cyclodextrin Bonded Stationary Phase Using Polar-Organic Acetonitrile as the Mobile Phase [J] . Chen Shushi Journal of the Chinese Chemical Society. . 1999,第2期

机译：使用极性有机乙腈作为流动相的＃beta＃-环糊精键合固定相上的苯甲酰基氨基酸，二肽和三肽的高效液相色谱对映体
3. Amino acid absorption and protein synthesis responses of turbot Scophthalmus maximus to lysine and leucine in free, dipeptide and tripeptide forms [J] . Journal of international management . 2020,第2期

机译：氨基酸吸收和蛋白质合成反应的混乱脱蛋白最大限度的自由，二肽和三肽形式的赖氨酸和亮氨酸
4. Fluoro-β-lactams as Useful Building Blocks for the Synthesis of Fluorinated Amino Acids, Dipeptides, and Taxoids [C] . Iwao Ojima, Larisa Kuznetsova, Ioana Maria Ungureanu, American Chemical Society Symposium on Fluorine-Containing Synthons . 2005

机译：氟-β-内酰胺作为合成氟化氨基酸，二肽和紫杉木的有用积木
5. Synthesis and enzymatic resolution of amino acid esters in "green" solvents: Ionic liquids. [D] . Zhao, Hua. 2002

机译：氨基酸酯在“绿色”溶剂中的合成和酶促拆分：离子液体。
6. The Proton Dissociation of Bio-Protic Ionic Liquids: AAEX Amino Acid Ionic Liquids [O] . Ting He, Cheng-Bin Hong, Peng-Chong Jiao, 2021

机译：生物保护离子液体的质子解离：X氨基酸离子液体
7. Luminescent dansyl-based ionic liquids from amino acids and methylcarbonate onium salt precursors: synthesis and photobehaviour [O] . Giulia Fiorani, Maurizio Selva, Alvise Perosa, 2015

机译：氨基酸和碳酸甲酯鎓盐前体的发光基于丹磺酰基的离子液体：合成和光行为

Coupling-Reagent-Free Synthesis of Dipeptides and Tripeptides Using Amino Acid Ionic Liquids

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