Efficient synthesis of manganese(II) carboxylates: from a trinuclear cluster [Mn_3(PhCO_2)_6(THF)_4] to a unique [Mn(PhCO_2)_2]_n chiral 3D network

Arkadiusz Kornowicz; Szymon Komorski; Zbigniew Wróbel; Iwona Justyniak; Natalia Nedelko; Anna ?lawska-Waniewska; Robert Balawender; Janusz Lewiński

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Efficient synthesis of manganese(II) carboxylates: from a trinuclear cluster [Mn_3(PhCO_2)_6(THF)_4] to a unique [Mn(PhCO_2)_2]_n chiral 3D network

机译：有效合成羧酸锰（II）：从三核簇[Mn_3（PhCO_2）_6（THF）_4]到独特的[Mn（PhCO_2）_2] _n手性3D网络

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An efficient synthetic procedure for obtaining manganese carboxylates including a trinuclear cluster [Mn_3(PhCO_2)_6(THF)_4]_2 and a unique [Mn(PhCO_2)_2]_n chiral 3D network is reported. The procedure involves a simple redox process, in which acidic protons are reduced to gaseous hydrogen by oxidizing metallic manganese under solvothermal conditions.

机译：报道了一种有效的合成程序，以获得包括三核簇[Mn_3（PhCO_2）_6（THF）_4] _2和独特的[Mn（PhCO_2）_2] _n手性3D网络的锰羧酸盐。该过程涉及简单的氧化还原过程，其中通过在溶剂热条件下氧化金属锰将酸性质子还原为气态氢。

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《Dalton transactions: An international journal of inorganic chemistry》 |2014年第8期|共4页
作者
Arkadiusz Kornowicz; Szymon Komorski; Zbigniew Wróbel; Iwona Justyniak; Natalia Nedelko; Anna ?lawska-Waniewska; Robert Balawender; Janusz Lewiński;
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正文语种 eng
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Efficient; synthesis; network;

机译：高效综合网络;

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1. Efficient synthesis of manganese(II) carboxylates: from a trinuclear cluster [Mn_3(PhCO_2)_6(THF)_4] to a unique [Mn(PhCO_2)_2]_n chiral 3D network [J] . Arkadiusz Kornowicz, Szymon Komorski, Zbigniew Wróbel, Dalton transactions: An international journal of inorganic chemistry . 2014,第8期

机译：有效合成羧酸锰（II）：从三核簇[Mn_3（PhCO_2）_6（THF）_4]到独特的[Mn（PhCO_2）_2] _n手性3D网络
2. [LnNa(PhCO_2)_4] (Ln = Ho, Dy): the first examples of chiral srs 3D networks constructed using the monotopic benzoate ligand [J] . Zeeshan Majeed, Kartik C. Mondal, George E. Kostakis, Chemical Communications . 2010,第15期

机译：[LnNa（PhCO_2）_4]（Ln = Ho，Dy）：使用单端苯甲酸酯配体构建的手性srs 3D网络的第一个示例
3. Synthesis, characterization and crystal structure of a new linear trinuclear manganese(II) complex, [Mn_3(PhCH=CHCO_2)_6(BPY)_2] centre dot H_2O (BPY = 2,2-bipyridine) [J] . YING CHEN, XIAN-WEN WANG, BO HU Journal of Coordination Chemistry . 2007,第22a24期

机译：新型线性三核锰（II）配合物[Mn_3（PhCH = CHCO_2）_6（BPY）_2]中心点H_2O（BPY = 2,2-Bipyridine）的合成，表征和晶体结构
4. Synthesis of a new pyridine-benzimidazole based ligand and application of its Ni(II) complex to the identification of chiral carboxylates [C] . Atsuko Kubota, Chihiro Abe, Hiroshi Katagiri 日本化学会春季年会講演予稿集 . 2018

机译：基于新的吡啶 - 苯并咪唑基配体的合成及其Ni（II）复合物在手性羧酸盐鉴定中的应用
5. Trinuclear rhenium(III) halide clusters with carboxylate ligands. [D] . Dougan, Jeffrey Steven. 2003

机译：三核rh（III）卤化物具有羧酸盐配体。
6. Synthesis Characterization and Oxygenation Studies of Carboxylate-Bridged Diiron(II) Complexes with Aromatic Substrates Tethered to Pyridine Ligands and the Formation of a Unique Trinuclear Complex [O] . Simone Friedle, Stephen J. Lippard -1

机译：用芳族底物拴在吡啶配体上的合成表征和氧合和氧合研究与吡啶配体的形成形成独特的三核络合物
7. Synthesis, Characterization, and Oxygenation Studies of Carboxylate-Bridged Diiron(II) Complexes with Aromatic Substrates Tethered to Pyridine Ligands and the Formation of a Unique Trinuclear Complex [O] . Friedle, Simone, Lippard, Stephen J. 2009

机译：羧酸盐桥联二铁（II）配合物的合成，表征和氧合研究，其中芳基底物与吡啶配体连接并形成独特的三核配合物

Efficient synthesis of manganese(II) carboxylates: from a trinuclear cluster [Mn_3(PhCO_2)_6(THF)_4] to a unique [Mn(PhCO_2)_2]_n chiral 3D network

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