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Facile fabrication and characterization of novel three-dimensional halloysite nanotubes/graphene oxide composite aerogels for waste water treatment

机译:浅塑造新型三维霍罗伊矿纳米管/石墨烯氧化物复合气凝胶的舒适制造与表征

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摘要

In order to develop efficient and environment benign sorbents for water purification, a simple hydrothermal process for fabrication of the halloysite (HNTs)/graphene oxide (GO) composite aerogels comprising HNTs anchored on graphene oxide sheets was developed. The morphology and structure of the materials were characterized by scanning electron microscopy (SEM), nitrogen adsorption-desorption, and Fourier transform infrared (FT-IR). The results demonstrated that the composites exhibit large surface area (S-BET = 361.3778m(2)g(-1)) and high pore volume (V-p = 1.2432cm(3)g(-1)) with only 10wt% of HNTs, higher than that of the ture GO aerogel (S-BET = 142.8816m(2)g(-1), V-p = 0.6106cm(3)g(-1)). The adsorption properties of the pure GO aerogels and n-HNTs/GO composite aerogels with 10wt% of n-HNTs were measured using a UV-Vis spectrophotometer. The results reflected that the adsorptivity of MB by the n-HNTs/GO composite aerogels was 99.3%, much higher than the pure GO aerogels (89.4%).
机译:为了开发有效和环境良性吸附剂进行净水,开发了一种简单的水热方法,用于制造锚定在石墨烯片上锚定的HNTS的霍罗伊矿(HNT)/石墨烯氧化物(GO)复合气凝胶。 通过扫描电子显微镜(SEM),氮吸附 - 解吸和傅立叶变换红外(FT-IR),表征了材料的形态和结构。 结果表明,复合材料表现出大的表面积(S-BET = 361.3778M(2)G(2)G(v))和高孔体积(VP = 1.2432cm(3)g(3)g(-1)),仅为10wt% 高于Ture Go气凝胶的HNT(S-BET = 142.816m(2)G(-1),VP = 0.6106cm(3)g(-1))。 使用UV-VIS分光光度计测量纯Go Aerogels和10wt%N-HNT的N-HNT /去复合气凝胶的吸附性能。 结果反映了N-HNT /去复合气凝胶的MB的吸附率为99.3%,远高于纯净气凝胶(89.4%)。

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