Syntheses, structures and magnetic properties of cyano-bridged (Fe2MII)-M-III (M = Mn, Co and Ni) one-dimensional chains

Wu Qiong; Meng Yin-Shan; Jiang Wen-Jing; Jiao Cheng-Qi; Liu Qiang; Zhu Hai-Lang; Liu Tao

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Syntheses, structures and magnetic properties of cyano-bridged (Fe2MII)-M-III (M = Mn, Co and Ni) one-dimensional chains

机译：氰基桥接（Fe2MII）-M-III（M = Mn，Co和Ni）一维链的合成，结构和磁性。一维链

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摘要

Three novel cyano-bridged one-dimensional chains {[(pzTp)Fe(CN)(3)](2) M(BYI)(2)(CH3OH)(2)center dot 2CH(3)OH](n), (M = Mn (1), Co (2) and Ni (3), BYI = 1, 1'-(1, 4-Butanediyl)bis(imidazole)) composed of cyano-bridged trinuclear (Fe2MII)-M-III units were successfully synthesized based on [(pzTp)Fe(CN)(3)](-) (pzTp = tetrakis(pyrazolyl)borate) unit and bidentate bridging ligand. Structural characterization showed that the three compounds were isostructural. The magnetic interactions could be adjusted by replacing the metal ions with different magnetic anisotropy. Magnetic studies revealed that compound 1 showed antiferromagnetic interaction, while compounds 2 and 3 exhibited ferromagnetic interaction. Interestingly, compound 3 showed the spin glass behavior with the typical slow magnetic relaxation due to the large anisotropy for Ni-II ions and the non-negligible interchain interaction.

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来源
《Inorganic Chemistry Communications》 |2018年第2018期|共5页
作者
Wu Qiong; Meng Yin-Shan; Jiang Wen-Jing; Jiao Cheng-Qi; Liu Qiang; Zhu Hai-Lang; Liu Tao;
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作者单位

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

Dalian Univ Technol State Key Lab Fine Chem Dalian 116024 Peoples R China;

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原文格式 PDF
正文语种 eng
中图分类无机化学;基本无机化学工业;
关键词
Cyano-bridged; One-dimensional chain; Building block; Magnetic interaction; Spin glass;

机译：氰桥;一维链;构建块;磁性相互作用;旋转玻璃;

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Syntheses, structures and magnetic properties of cyano-bridged (Fe2MII)-M-III (M = Mn, Co and Ni) one-dimensional chains

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