A new functionalized POM-based MOF containing 1D [Mo3O10](n)(2n-) chains and the flexible bis(pyrazine)-bis(amide) ligand

Cui Ziwei; Lin Hongyan; Zeng Ling; Lu Junjun

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A new functionalized POM-based MOF containing 1D [Mo3O10](n)(2n-) chains and the flexible bis(pyrazine)-bis(amide) ligand

机译：含有1D [Mo3O10]（N）链和柔性双（吡嗪） - 基（酰胺）配体的新官能化POM基础MOF

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摘要

A new 3D metal?organic framework (MOF) derived from the 1D [Mo3O10](n)(2n-) chains and the flexible N,N'-bis(5-methyl-2-pyrazinecarboxamide)-1,2-ethane (bmpae), [Cu(bmpae)(0.5)(Mo3O10)(H2O)]center dot H2O (1) has been hydro-thermally synthesized. Crystal analysis reveals that complex 1 is a 3D polyoxometalate (POM)-based MOF containing the 2D [Cu(bmpae)(0.5)](n)(2n+) metal-organic layers and the 1D inorganic [Mo3O10](n)(2n-) chains. The electrochemical behaviors and electrochemical sensing property of the title complex were studied, and its adsorption capacities towards organic dyes gentian violet (GV) and methylene blue (MB) were also investigated.

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来源
《Inorganic Chemistry Communications》 |2021年第1期|共5页
作者
Cui Ziwei; Lin Hongyan; Zeng Ling; Lu Junjun;
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作者单位

Bohai Univ Coll Chem &

Mat Engn Liaoning Profess Technol Innovat Ctr Liaoning Pro Jinzhou 121013 Peoples R China;

Bohai Univ Coll Chem &

Mat Engn Liaoning Profess Technol Innovat Ctr Liaoning Pro Jinzhou 121013 Peoples R China;

Bohai Univ Coll Chem &

Mat Engn Liaoning Profess Technol Innovat Ctr Liaoning Pro Jinzhou 121013 Peoples R China;

Bohai Univ Coll Chem &

Mat Engn Liaoning Profess Technol Innovat Ctr Liaoning Pro Jinzhou 121013 Peoples R China;

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原文格式 PDF
正文语种 eng
中图分类无机化学;基本无机化学工业;
关键词
Polyoxomolybdate; Bis(pyrazine)-bis(amide) ligand; Metal-organic framework; Electrochemical sensor; Adsorption property;

机译：聚氧化钼酸盐;双（吡嗪）-BIS（酰胺）配体;金属有机框架;电化学传感器;吸附性质;

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1. Evans-Showell-type polyoxometalate-based metal-organic complexes with novel 3D structures constructed from flexible bis-pyrazine-bis-amide ligands and copper metals: syntheses, structures, and fluorescence and catalytic properties [J] . Li Feng-Cai, Li Xi-Li, Tan Li-Kun, Dalton transactions: An international journal of inorganic chemistry . 2019,第6期

机译：evans-showell型聚杂物酸酯基金属 - 有机配合物，具有由柔性双吡嗪 - 双酰胺配体和铜金属构成的新型3D结构：合成，结构和荧光和催化性能
2. Application of flexible bis-pyrazine-bis-amide ligands to construct various polyoxometalate-based metal-organic complexes [J] . Wang Xiu-Li, Liu Dan-Na, Lin Hong-Yan, RSC Advances . 2015,第70期

机译：柔性双吡嗪 - 双酰胺配体的应用构建各种聚氧酸盐基金属 - 有机络合物
3. Two isostructural 3D metal-organic frameworks constructed from ID [H2Mo4O_(14)]n~(2n) chains and the flexible bis-pyridyl-bis-amide ligand [J] . Hongyan Lin, Chuang Xu, Xiuli Wang Inorganic Chemistry Communications . 2013,第Null期

机译：由ID [H2Mo4O_（14）] n〜（2n）链和柔性双吡啶基-双酰胺配体构成的两个同构3D金属-有机骨架
4. DESIGN AND SYNTHESIS OF ISONIAZIDE MIMETIC CONJUGATED WITH DTPA, POTENTIAL LIGAND OF NOVEL RADIOPHARMACEUTICAL AND CONTRAST AGENT FOR MEDICAL IMAGING BIS (AMIDE) OF DIETHYLENETRIAMINEPENTAACETIC ACID: DTPA-BIS(INH) [C] . A.K. MISHRA, P. PANWAR, K. CHUTTANI, Trends in Radiopharmaceuticals(ISTR-2005) . 2007

机译：DTPA，新型放射性药物的潜在配体和二乙二胺戊酸医学影像双（酰胺）造影剂的潜在配位体的合成方法
5. Tridentate nitrogen ligands derived from 2,6-bis-hydrazinopyridine (BHP): Preparation and study of the 2,6-bis-hydrazonopyridines, 2,6-bis-pyrazolylpyridines, and 2,6-bis-indazolylpyridines. [D] . Duncan, Nathan C. 2009

机译：源自2,6-双-肼基吡啶（BHP）的三齿氮配体：2,6-双-肼基吡啶，2,6-双-吡唑基吡啶和2,6-双-吲唑基吡啶的制备和研究。
6. A Pair of CoII Supramolecular Isomers Based on Flexible Bis-Pyridyl-Bis-Amide and Angular Dicarboxylate Ligands [O] . Pradhumna Mahat Chhetri, Ming-Hao Wu, Chou-Ting Hsieh, 2020

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机译：一种基于柔性双吡啶基 - 双酰胺配体的新型3D滤蛋白金属 - 有机框架
8. Organic Main-Chain NLO Polymers. 1. Copolymerization of Bis(arylcarboxaldehyde) and Bis(cyanoacetate) Monomers via the Knoevenagel Condensation. [R] . Wright, M. E., Mullick, S. 1992

机译：有机主链NLO聚合物。 1.通过Knoevenagel缩合共聚合双（芳基甲醛）和双（氰基乙酸酯）单体。

A new functionalized POM-based MOF containing 1D [Mo3O10](n)(2n-) chains and the flexible bis(pyrazine)-bis(amide) ligand

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