Poly(butylene adipate-co-terephthalate) Polyester Synthesis Process and Product Development

Mahata Denial; Karthikeyan Sangeetha; Godse Rahul; Gupta Virendra Kumar

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Poly(butylene adipate-co-terephthalate) Polyester Synthesis Process and Product Development

机译：聚（丁烯己二酸丁二醇酯）聚酯合成过程和产品开发

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摘要

Poly(butylene adipate-co-terephthalate) is a well-known aliphatic-aromatic biodegradable random co-polyester that is structurally composed of a chemical unit of butylene adipate and butylene terephthalate. It can be synthesized by a polycondensation reaction in the melt stage. However, the synthesis process is very much complicated because it requires a high esterification temperature as well as a vacuum to achieve a suitable molecular weight for different grade industrial applications. Additionally, the synthesis process gives the various side reactions that associate depolymerization with hydrolytic degradation, the color of polymer, tetrahydrofuran formation, etc. This short literature review deals with the various methods development of poly(butylene adipate-co-terephthalate) synthesis for commercial scale. Moreover, different grades of its synthesis are also investigated with chain extenders, branching agents, chemical functionalization and in-situ incorporation of nanocomposites.

机译：聚（己二酸丁二醇酯-对苯二甲酸共酯）是一种众所周知的脂肪族芳香族可生物降解无规共聚酯，其结构由己二酸丁二醇酯和对苯二甲酸丁二醇酯的化学单元组成。它可以在熔融阶段通过缩聚反应合成。然而，合成过程非常复杂，因为它需要较高的酯化温度和真空，以获得适合不同等级工业应用的合适分子量。此外，合成过程还产生了各种副反应，这些副反应将解聚与水解降解、聚合物的颜色、四氢呋喃的形成等联系在一起。这篇简短的文献综述介绍了商业规模的聚己二酸丁二醇酯-对苯二甲酸乙二酯合成的各种方法。此外，还研究了扩链剂、支化剂、化学功能化和纳米复合材料原位掺入对其合成的影响。

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《Polymer science, Series C》 |2021年第1期|共10页
作者
Mahata Denial; Karthikeyan Sangeetha; Godse Rahul; Gupta Virendra Kumar;
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作者单位

Reliance Ind Ltd Reliance Res &

Dev Ctr Polymer Synth &

Catalysis Grp Navi Mumbai 400701 India;

Reliance Ind Ltd Reliance Res &

Dev Ctr Polymer Synth &

Catalysis Grp Navi Mumbai 400701 India;

Reliance Ind Ltd Reliance Res &

Dev Ctr Polymer Synth &

Catalysis Grp Navi Mumbai 400701 India;

Reliance Ind Ltd Reliance Res &

Dev Ctr Polymer Synth &

Catalysis Grp Navi Mumbai 400701 India;

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正文语种 eng
中图分类有机化学;
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1. Synthesis and Characterization of Poly（butylene adipate-co-terephthalate） Catalyzed by Rare Earth Stearates [J] . 朱魁, 朱蔚璞, 顾燕波, 中国化学：英文版 . 2007,第010期
2. Poly(Butylene Adipate-Co-Terephthalate)and Poly(ε-Caprolactone)and Their Bionanocomposites with Cellulose Nanocrystals:Thermo-Mechanical Properties and Cell Viability Study [J] . Marcia Cristina Branciforti, Caroline Faria Bellani, Carolina Lipparelli Morelli, 可再生材料杂志(英文) . 2019,第003期
3. Nonisothermal Crystallization Kinetics of Poly(butylene adipate-co-terephthalate) Copolyester [J] . Wang Xiaohui, Shi Jun, Chen Ying, 中国炼油与石油化工（英文版） . 2012,第001期
4. INVESTIGATION ON THE GELATION BEHAVIOR OF BIODEGRADABLE POLY（BUTYLENE SUCCINATE） DURING ISOTHERMAL CRYSTALLIZATION PROCESS [J] . Fa-liang Luo, Xiu-qin Zhang, Wei Ning, 高分子科学：英文版 . 2011,第002期
5. Synthesis and Properties of Poly(butylene carbonate-co-spirocyclic carbonate) [J] . ZHU Changliang, LIU Shaoying, WANG Qingyin, 高等学校化学研究（英文版） . 2019,第004期
6. Structure development and properties of high-speed melt spun poly(butylene terephthalate)/poly(butylene adipate-co-terephthalate) bicomponent fibers [J] . Shi XQ, Ito H, Kikutani T Polymer: The International Journal for the Science and Technology of Polymers . 2006,第2期

机译：高速熔纺聚对苯二甲酸丁二醇酯/聚己二酸丁二醇酯-对苯二甲酸对苯二甲酸丁二酯双组分纤维的结构发展和性能
7. Synthesis of Bio-Nanomagnetite Using Poly(butylene adipate) and Poly(butylene adipate-co-terephthalate) [J] . Hosseini F., Eshaghi Z. Journal of inorganic and organometallic polymers and materials . 2020,第11期

机译：使用聚（丁烯己二酸丁酯）和聚（丁烯己二酸丁二醇酯 - 对苯二甲酸丁酯的生物纳米磁石合成
8. Effect of nanofillers characteristics and their selective localization on morphology development and rheological properties of melt-processed polylactide/poly(butylene adipate-co-terephthalate) blend composites [J] . Salehiyan Reza, Nofar Mohammadreza, Malkappa Kuruma, Polymer engineering and science . 2020,第11期

机译：纳米填料特征的影响及其选择性定位对熔融加工聚物/聚（丁烯己二酸丁二醇酯）混合复合材料的形态发育和流变性能
9. Synthesis, Structure and Properties on Biodegradable Polyesters of Poly(Butylenes Adipic-co-butylene Terephthalate) Catalyzed by Organic Rare Earth Compound [C] . The 12th Asian Pacific Confederation of Chemical Engineering Congress(第十二届亚太化工联盟大会暨化工展览会)论文集 . 2008

机译：有机稀土化合物催化的聚对苯二甲酸丁二酯-对苯二甲酸丁二醇酯的可生物降解聚酯的合成，结构和性能
10. The synthesis and development of novel, easily processable poly (n-isopropylacrylamide)-based hyrdogels [D] . Boyes, Victoria L. 2012

机译：新颖，易加工的聚（N-异丙基丙烯酰胺）的合成和发展 - 基于肝脏的Hyrdogels
11. Development of Toughened Flax Fiber Reinforced Composites. Modification of Poly(lactic acid)/Poly(butylene adipate-co-terephthalate) Blends by Reactive Extrusion Process [O] . Jacek Andrzejewski, Michał Nowakowski 2021

机译：强化亚麻纤维增强复合材料的研制。通过反应挤出法对聚（乳酸）/聚（丁烯己二酸丁二醇酯）共混物的改性
12. Development of Toughened Blends of Poly(lactic acid) and Poly(butylene adipate-co-terephthalate) for 3D Printing Applications: Compatibilization Methods and Material Performance Evaluation [O] . -1

机译：用于3D印刷应用的聚（乳酸）和聚（丁烯己二酸丁二醇酯 - 对苯二甲酸丁二醇酯）的增韧混合物的发展：相容方法和材料性能评估
13. New Processable Poly(ether-Keto-Sulfone)s, Poly(arylene Sulfone)s, and Polyesters Curable by Intramolecular Cyclization. XVII [R] . Somers, A., Marvel, C. S. 1979

机译：新型可加工聚（醚 - 酮 - 砜），聚（亚芳基砜）和可通过分子内环化合成的聚酯。 XVII

Poly(butylene adipate-co-terephthalate) Polyester Synthesis Process and Product Development

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