High-pressure synthesis and crystal structure of α-Y2B4O9

Martin K.Schmitt; HubertHuppertz

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High-pressure synthesis and crystal structure of α-Y2B4O9

机译：α-Y2B4O9的高压合成和晶体结构

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α-Y2B4O9 was synthesized in a high-pressure/high-temperature experiment at 12.3 GPa/1020°C. The crystal structure has been determined via single-crystal X-ray diffraction. α-Y2B4O9 is isotypic to the lanthanide borates α-Ln2B4O9 (Ln=Sm–Ho) and crystallizes in the monoclinic space group C2/c (no. 15) with the following lattice parameters: a=25.084(2), b=4.3913(2), c=24.726(2) ?, and β=99.97(1)°. The compound was further characterized via X-ray powder diffraction as well as IR and Raman spectroscopy.

机译：在12.3 GPa/1020°C的高压/高温实验中合成了α-Y2B4O9。通过单晶X射线衍射确定了晶体结构。α-Y2B4O9与镧系硼酸盐α-Ln2B4O9（Ln=Sm–Ho）同构，在单斜空间群C2/c（no.15）中结晶，晶格参数如下：a=25.084（2），b=4.3913（2），c=24.726（2）？，β=99.97（1）°。通过X射线粉末衍射、红外光谱和拉曼光谱对化合物进行了进一步表征。

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来源
《Zeitschrift fur Naturforschung, B. A Journal of Chemical Sciences》 |2017年第12期|共6页
作者
Martin K.Schmitt; HubertHuppertz;
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作者单位

Institut für Allgemeine Anorganische und Theoretische Chemie Universit?t Innsbruck Innrain 80–82 6020 Innsbruck Austria;

Institut für Allgemeine Anorganische und Theoretische Chemie Universit?t Innsbruck Innrain 80–82 6020 Innsbruck Austria Fax: +43 (512) 507-57099;

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正文语种 eng
中图分类化学;
关键词
crystal structure; high-pressure chemistry; vibrational spectroscopy; yttrium borate;

机译：晶体结构;高压化学;振动光谱;YTTRIUM BORATE;

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High-pressure synthesis and crystal structure of α-Y2B4O9

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