Topochemical polymerization of macrocyclic diacetylene with a naphthalene moiety for a tubular-shaped polydiacetylene chromophore

Kantha Chandra; Kim Hansol; Kim Youngmee; Heo Jung-Moo; Joung Joonyoung F.; Park Sungnam; Kim Jong-Man

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Topochemical polymerization of macrocyclic diacetylene with a naphthalene moiety for a tubular-shaped polydiacetylene chromophore

机译：用萘部分的大环二乙炔为管状多二亚二乙烯发色团的大环二乙烯的类别化学聚合

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摘要

Tubular-shaped chromophores have great potential in chemical and material sciences. A naphthalene-containing macrocyclic diacetylene (MCDA-Naph) was synthesized to access covalently linked organic nanotubes (ONTs) through topochemical polymerization. Single crystal X-ray analysis revealed that MCDA-Naph adopts the desired tubular array with favorable molecular orientation. UV irradiation of the molecularly stacked MCDA-Naph resulted in 1,4-addition polymerization and the generation of conjugated ene-yne chromophores. Density functional theory (DFT) provided evidence for tubular polydiacetylene nanotubes.

机译：管状发色团在化学和材料科学中具有巨大的潜力。合成了一种含萘的大环二乙炔（MCDA-Naph），通过拓扑化学聚合获得共价连接的有机纳米管（ONT）。单晶X射线分析表明，MCDA Naph采用了理想的管状阵列，具有良好的分子取向。紫外辐照分子堆积的MCDA Naph导致1,4-加成聚合和共轭烯炔生色团的产生。密度泛函理论（DFT）为管状聚二乙炔纳米管提供了证据。

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来源
《Dyes and Pigments》 |2018年第2018期|共6页
作者
Kantha Chandra; Kim Hansol; Kim Youngmee; Heo Jung-Moo; Joung Joonyoung F.; Park Sungnam; Kim Jong-Man;
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作者单位

Hanyang Univ Inst Nano Sci &

Technol Seoul 04763 South Korea;

Hanyang Univ Dept Chem Engn Seoul 04763 South Korea;

Ewha Womans Univ Inst Nanobio Technol Seoul 03760 South Korea;

Hanyang Univ Dept Chem Engn Seoul 04763 South Korea;

Korea Univ Dept Chem Seoul 02841 South Korea;

Korea Univ Dept Chem Seoul 02841 South Korea;

Hanyang Univ Inst Nano Sci &

Technol Seoul 04763 South Korea;

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原文格式 PDF
正文语种 eng
中图分类染料及中间体工业;颜料工业;
关键词
Polydiacetylene; Macrocyclic diacetylene; Conjugated polymer; Chromophore; Topochemical polymerization;

机译：多二乙烯;大环二乙烯;共轭聚合物;发色团;Topochemical聚合;

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2. Interlayer Energy Transfer from Naphthalene to Anthracene Chromophores Organized in Langmuir—Blodgett Films [J] . LiQianLI, ChiMingCHE, 等中国化学快报：英文版 . 2002,第001期
3. Interlayer Energy Transfer from Naphthalene to Anthracene Chromophores Organized in Langmuir-Blodgett Films [J] . 中国化学快报（英文版） . 2002,第001期
4. Topochemical polymerization of macrocyclic diacetylene with a naphthalene moiety for a tubular-shaped polydiacetylene chromophore [J] . Kantha Chandra, Kim Hansol, Kim Youngmee, Dyes and Pigments . 2018,第期

机译：用萘部分的大环二乙炔为管状多二亚二乙烯发色团的大环二乙烯的类别化学聚合
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机译：大环二乙炔 - 立噻吩cocrystal：分子自组装，类别化学聚合和能量转移
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7. Synthesis, Characterization and Ring-opening Polymerization of Macrocyclic Aryl Ketone Oligomers Containing the Phthaloyl Moiety [C] . HU Li-song, GUO Qing-zhong 2013 International conference on process equipment, mechatronics engineering and material science . 2013

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8. I. Topochemical polymerization of novel diacetylenes. II. Synthesis and characterizations of soluble polydiacetylenes [D] . Li, Zhong 2008

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9. Polymers with advanced structural and supramolecular features synthesized through topochemical polymerization [O] . Kuntrapakam Hema, *, Arthi Ravi, 2021

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10. Chromogenic Tubular Polydiacetylenes from Topochemical Polymerization of Self-Assembled Macrocyclic Diacetylenes [O] . -1

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机译：含有两个α，α'-双（氨基甲基）吡啶部分的（30）py2N4O4大环配体的双核配合物。与类似的22和24元大环配体的比较。

Topochemical polymerization of macrocyclic diacetylene with a naphthalene moiety for a tubular-shaped polydiacetylene chromophore

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