One-pot synthesis of 3D-ZIF-7 supported on 2D-Zn-Benzimidazole-Acetate and its catalytic activity in the methoxycarbonylation of aniline with dimethyl carbonate

Dahnum Deliana; Dang Huyen Tran; Tran Ngoc Tuan; Ha Jeong-Myeong; Lee Hyunjoo

首页> 外文期刊>Journal of industrial and engineering chemistry >One-pot synthesis of 3D-ZIF-7 supported on 2D-Zn-Benzimidazole-Acetate and its catalytic activity in the methoxycarbonylation of aniline with dimethyl carbonate

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One-pot synthesis of 3D-ZIF-7 supported on 2D-Zn-Benzimidazole-Acetate and its catalytic activity in the methoxycarbonylation of aniline with dimethyl carbonate

机译：用二甲基甲酸二甲基苯甲酸甲氧基羰基化的3D-ZIF-7支持3D-ZIF-7的合成及其催化活性

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摘要

For the first time, three-dimensional Zeolitic Imidazole Framework (3D) ZIF-7 (Zn(BeIM)(2), BeIM = benzimidazole) supported on two-dimensional (2D) Zn(BeIM)OAc (Zinc-Benzimidazole-Acetate) was synthesized by reacting Zn(OAc)(2) and benzimidazole in a one-pot reaction. By modulating the amount of diethylamine during the reaction, the ZIF-7/Zn(BeIM)OAc with a 1 to 1 molar ratio was obtained when the reactant molar ratio of Zn(OAc)(2) and benzimidazole was 1 to 1.5. It was found that 3D-ZIF-7 was synthesized first and then transformed into 2D-Zn(BeIM)OAc by the reaction with remaining Zn(OAc)(2).

机译：通过锌（OAc）（2）与苯并咪唑的一锅反应，首次合成了以二维锌（BeIM）OAc（苯并咪唑乙酸锌）为载体的三维沸石咪唑骨架ZIF-7（Zn（BeIM）（2），BeIM=苯并咪唑）。通过调节反应过程中二乙胺的用量，当锌（OAc）（2）与苯并咪唑的摩尔比为1:1.5时，可得到摩尔比为1:1的ZIF-7/Zn（BeIM）OAc。研究发现，3D-ZIF-7首先被合成，然后通过与剩余的锌（OAc）反应转化为2D Zn（BeIM）OAc（2）。

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来源
《Journal of industrial and engineering chemistry》 |2021年第1期|共8页
作者
Dahnum Deliana; Dang Huyen Tran; Tran Ngoc Tuan; Ha Jeong-Myeong; Lee Hyunjoo;
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作者单位

Korea Inst Sci &

Technol Clean Energy Res Ctr 5 Hwarang Ro 14 Gil Seoul 02792 South Korea;

Korea Inst Sci &

Technol Clean Energy Res Ctr 5 Hwarang Ro 14 Gil Seoul 02792 South Korea;

Korea Inst Sci &

Technol Clean Energy Res Ctr 5 Hwarang Ro 14 Gil Seoul 02792 South Korea;

Korea Inst Sci &

Technol Clean Energy Res Ctr 5 Hwarang Ro 14 Gil Seoul 02792 South Korea;

Korea Inst Sci &

Technol Clean Energy Res Ctr 5 Hwarang Ro 14 Gil Seoul 02792 South Korea;

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原文格式 PDF
正文语种 eng
中图分类化学工业;
关键词
ZIF-7; Zn(BeIM)OAc; One-pot synthesis; Methoxycarbonylation;

机译：None;

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One-pot synthesis of 3D-ZIF-7 supported on 2D-Zn-Benzimidazole-Acetate and its catalytic activity in the methoxycarbonylation of aniline with dimethyl carbonate

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