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Effect of 2 wt.% Addition of Fe on the Compressive Properties and Corrosion Behavior of Zn-HAp-Fe Material

机译:2重量%的效果。Zn-Hap-Fe材料的压缩性能和腐蚀行为的效果

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The present work deals in developing new zinc-based composite material for bone repair using a powder metallurgy process. Zinc (Zn), hydroxyapatite (HAp), and iron (Fe) powders were mechanically mixed with ball milling. Subsequently, the powder mixture was compacted to form the green compact. After that, the green compacts were sintered using a microwave sintering furnace. The mechanical and electrochemical behaviors of the prepared Zn-based samples were tested as per the standards. X-ray diffraction and energy-dispersive spectroscopic examinations revealed the existence of HAp and Fe in the Zn matrix. The compressive yield strength and compressive strength of the developed Zn-5HAp-2Fe material were found to be 117.91 +/- 7.42 and 170.87 +/- 7.41 MPa, respectively. In vitro electrochemical corrosion analysis of the developed Zn-5HAp-2Fe sample in simulated body fluid solution unveiled the corrosion rate as 0.116 +/- 0.021 mm center dot year(-1). The mechanical and degradation behaviors of Zn-5HAp-2Fe material showed the potential to be used as a bone fixation material.
机译:目前的工作涉及使用粉末冶金工艺开发用于骨修复的新型锌基复合材料。锌(Zn)、羟基磷灰石(HAp)和铁(Fe)粉末通过球磨进行机械混合。随后,粉末混合物被压实以形成绿色压实体。之后,使用微波烧结炉烧结生坯。按照标准测试了制备的锌基样品的力学和电化学行为。X射线衍射和能量色散光谱检查表明,锌基体中存在HAp和Fe。开发的Zn-5HAp-2Fe材料的压缩屈服强度和压缩强度分别为117.91+/-7.42和170.87+/-7.41 MPa。对开发的Zn-5HAp-2Fe样品在模拟体液溶液中的体外电化学腐蚀分析显示,腐蚀速率为0.116+/-0.021 mm中心点年(-1)。Zn-5HAp-2Fe材料的力学性能和降解性能显示出其作为骨固定材料的潜力。

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