Halogen-Bonded Organic Frameworks of Perfluoroiodo- and Perfluorodiiodobenzene with 2,2′,7,7′-Tetrapyridyl-9,9′-spirobifluorene

Lidia  Pop; Ioana Georgeta  Grosu; Maria  Micl?u?; Niculina Daniela  H?dade; Alexandra  Pop; Attila  Bende; Anamaria  Terec; Mihail  Barboiu; Ion  Grosu

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Halogen-Bonded Organic Frameworks of Perfluoroiodo- and Perfluorodiiodobenzene with 2,2′,7,7′-Tetrapyridyl-9,9′-spirobifluorene

机译：全氟二核和全氟二苯苯苯苯并卤代的有机骨架，具有2,2'，7,7'-四吡啶基-9,9,9'-螺氟芴

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Single-crystal X-ray diffraction studies on Halogen-Bonded Organic Frameworks (XBOF) formed by N---I contacts of 2,2′,7,7′-tetrapyridyl-9,9′-spirobifluorene with pentafluoroiodobenzene or the isomers of diiodotetrafluorobenzene revealed the formation by F---I, F---F, and I---I halogen bonds of unique tetrameric superstructures of the halogenated derivatives in which the position of I atoms is mimicking the orientation of pyridyl groups in the 9,9′-spirobifluorene derivative resulting in the 1/4 molar ratio coordination of the halogenated compounds to the tetrapyridyl spiro derivative.

机译：对2,2′，7,7′-四吡啶基-9,9′-螺二芴与五氟碘苯或二碘四氟苯异构体的N---I接触形成的卤素键合有机框架（XBOF）的单晶X射线衍射研究表明，F---I，F---F，卤化衍生物独特的四聚体超结构的I---I卤素键，其中I原子的位置模拟9,9′-螺二芴衍生物中吡啶基的取向，从而导致卤化化合物与四吡啶基螺环衍生物的1/4摩尔比配位。

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《Crystal growth & design》 |2021年第2期|共10页
作者
Lidia Pop; Ioana Georgeta Grosu; Maria Micl?u?; Niculina Daniela H?dade; Alexandra Pop; Attila Bende; Anamaria Terec; Mihail Barboiu; Ion Grosu;
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Faculty of Chemistry and Chemical Engineering Department of Chemistry and SOOMCC Babes-Bolyai University;

National Institute for Research and Development of Isotopic and Molecular Technologies;

National Institute for Research and Development of Isotopic and Molecular Technologies;

Faculty of Chemistry and Chemical Engineering Department of Chemistry and SOOMCC Babes-Bolyai University;

Faculty of Chemistry and Chemical Engineering Department of Chemistry and SOOMCC Babes-Bolyai University;

National Institute for Research and Development of Isotopic and Molecular Technologies;

Faculty of Chemistry and Chemical Engineering Department of Chemistry and SOOMCC Babes-Bolyai University;

ENSCM-UM-CNRS UMR-5635 Institut Européen des Membranes University of Montpellier;

Faculty of Chemistry and Chemical Engineering Department of Chemistry and SOOMCC Babes-Bolyai University;

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正文语种 eng
中图分类晶体学;
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机译：包含9,9'-螺二芴的层状化合物：由9,9'-螺二芴-2,2'，7,7'-四羧酸衍生的氢键和金属有机网络
2. Theoretical design and simulations of hole transporting materials based on 2,2 ',7,7 '-tetrakis(N,N-di-p-methoxyphenyl-amine)9,9 '-spirobifluorene for organic-inorganic hybrid perovskite solar cells [J] . Zhang Bing, Xu Yingxue, Yang Jieqin, Computational & theoretical chemistry . 2019,第期

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机译：改进的2,2'-二溴-9,9'-螺双芴及其2,2'-Bisdonor-7,7'-双受体取代的荧光衍生物的合成
4. Organic room-temperature phosphorescence from halogen-bonded organic frameworks: hidden electronic effects in rigidified chromophores [O] . Jiawang Zhou, Ljiljana Stojanović, Andrey A. Berezin, 2021

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5. 2,2′,7,7′-Tetrabromo-9,9′-spirobifluorene toluene hemisolvate [O] . Ailing Guo, Ruitao Zhu 2009

机译：2,2＆amp;＃8242;，7,7＆amp;＃8242; -Tetrabromo-9,9＆amp;＃8242; -spirobifluorene甲苯半溶剂化物

Halogen-Bonded Organic Frameworks of Perfluoroiodo- and Perfluorodiiodobenzene with 2,2′,7,7′-Tetrapyridyl-9,9′-spirobifluorene

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