Solid-phase synthesis of recyclable diphosphine ligands

Heutz Frank J. L.; Samuels Michiel C.; Kamer Paul C. J.

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Solid-phase synthesis of recyclable diphosphine ligands

机译：可回收双磷酸配体的固相合成

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摘要

An efficient solid-phase synthetic approach towards diphosphine ligands is demonstrated. This modular method offers facile access to this important class of ligands, in quantitative yield, providing huge potential for ligand fine-tuning. These supported ligands can be efficiently applied in asymmetric catalysis. Moreover, the immobilized catalysts can successfully be recycled multiple times addressing several synthetic and work-up challenges in the field of catalytic chemistry.

机译：已经证明了对双磷酸配体的有效固相合成方法。这种模块化方法可轻松访问这一重要的配体，以定量的产量，为配体微调提供了巨大的潜力。这些支持的配体可以有效地应用于不对称催化中。此外，固定的催化剂可以多次成功地回收，以解决催化化学领域的几个合成和锻炼挑战。

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来源
《Catalysis science & technology》 |2015年第6期|3296-3301|共6页
作者
Heutz Frank J. L.; Samuels Michiel C.; Kamer Paul C. J.;
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作者单位

Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland;

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原文格式 PDF
正文语种英语
中图分类汉语教学;
关键词
SYNTHETICS; Solid-Phase Synthesis; asymmetric catalysis;

机译：合成;固相合成;不对称催化;

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1. Synthesis of a highly hydrophobic cyclic decapeptide by solid-phase synthesis of linear peptide and cyclization in solution [J] . Jian Chen, Bei Zhang, Cao Xie, 中国化学快报（英文版） . 2010,第4期
2. Erratum: Reactivity of dipyridyl ditellurides with (diphosphine)Pt ~0 and 2-pyridyltellurolates with (diphosphine)PtCl _2 and isolation of different structural motifs of platinum(II) complexes (Organometallics (2012) 31:5 (1743-1750) DOI: 10.1021/om2010589) (Erratum) [J] . Chauhan R.S., Kedarnath G., Wadawale A., Organometallics . 2012,第10期

机译：勘误表：二吡啶基二碲化物与（diphosphine）Pt〜0的反应性和2-吡啶基碲酸盐与（diphosphine）PtCl _2的反应以及铂（II）配合物不同结构图案的分离（Organometallics（2012）31：5（1743-1750）DOI： 10.1021 / om2010589）（勘误表）
3. Reactivity of dipyridyl ditellurides with (diphosphine)Pt ~0 and 2-pyridyltellurolates with (diphosphine)PtCl _2 and isolation of different structural motifs of platinum(II) complexes [J] . Chauhan R.S., Kedarnath G., Wadawale A., Organometallics . 2012,第5期

机译：二吡啶基二碲化物与（diphosphine）Pt〜0的反应性和2-吡啶基碲酸盐与（diphosphine）PtCl _2的反应以及铂（II）配合物不同结构图案的分离
4. Erratum: Reactivity of dipyridyl ditellurides with (diphosphine)Pt ~0 and 2-pyridyltellurolates with (diphosphine)PtCl _2 and isolation of different structural motifs of platinum(II) complexes (Organometallics (2012) 31:5 (1743-1750) DOI: 10.1021/om2010589) (Erratum) [J] . Chauhan R.S., Kedarnath G., Wadawale A., Organometallics . 2012,第10期

机译：勘误表：二吡啶基二碲化物与（diphosphine）Pt〜0的反应性和2-吡啶基碲酸盐与（diphosphine）PtCl _2的反应以及铂（II）配合物不同结构图案的分离（Organometallics（2012）31：5（1743-1750）DOI： 10.1021 / om2010589）（勘误表）
5. Synthesis and Characterization of YAG:Ce Phosphor by Microwave Induced Combustion Synthesis with Different Fuel Sources [C] . Khai Shenn Lau, Zainuriah Hassan, Way Foong Lim, International Conference on Semiconductor Materials and Technology . 2019

机译：Synthesis and Characterization of YAG:Ce Phosphor by Microwave Induced Combustion Synthesis with Different Fuel Sources
6. I. Symmetrical ligand bridged bimetallic complexes of rhenium(I): Implications for electrocatalytic reduction of carbon dioxide. II. Unimolecular excited state relaxation pathways in polypyridyl complexes of rhenium(I). [D] . Baiano, John Augustus. 1992

机译：I. ligand的对称配体桥联双金属络合物（I）：对电催化还原二氧化碳的影响。二。 poly（I）聚吡啶配合物中的单分子激发态弛豫途径。
7. Synthesis and cyclic voltammetric studies of diiron complexes ER2(η5-C5H4)Fe(L2)Me2 (E = C Si Ge Sn; R = H alkyl; L2 = diphosphine and (η5-C5H5)Fe(L2)ER2Fc Fc = (η5-C5H4)Fe(η5-C5H5) [O] . Mukesh Kumar, Francisco Cervantes-Lee, Keith H. Pannell, -1

机译：二铁配合物ER2 （（η5-C5H4）Fe（L2）Me 2（E = CSiGeSn; R = H烷基; L2 = diphosphine和（η5-C5H5）的合成及循环伏安研究Fe（L2）ER2Fc Fc =（η5-C5H4）Fe（η5-C5H5）
8. Adventure in Asymmetric Hydrogenation:Synthesis of Chiral Phosphorus Ligands and Asymmetric Hydrogenation of Heteroaromatics [O] . 胡向平, 王躲生, 余长斌, 2011

机译：adventure in asymmetric Hydrogenation:synthesis of Chiral phosphorus Ligands and asymmetric Hydrogenation of Heteroaromatics
9. Ligand Field Millimeter Maser [R] . Naiman, C. S., Schwartz, J., Linz, A. 1966

机译：Ligand Field millimeter maser

Solid-phase synthesis of recyclable diphosphine ligands

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