An in situ acidic carbon dioxide/glycol system for aerobic oxidative iodination of electron-rich aromatics catalyzed by Fe(NO3)(3).9H(2)O

Ma Ran; Huang Cheng-Bin; Liu An-HuaLi Xue-DongHe Liang-Nian

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An in situ acidic carbon dioxide/glycol system for aerobic oxidative iodination of electron-rich aromatics catalyzed by Fe(NO3)(3).9H(2)O

机译：原位酸性二氧化碳/乙二醇系统，用于用Fe（NO3）（3）（3）（2）O

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摘要

An environmentally benign CO2/glycol reversible acidic system was developed for the iron(III)-catalyzed aerobic oxidative iodination of electron-rich aromatics without the need for any conventional acid additive or organic solvent. Notably, moderate to high isolated yields (up to 97%) of the aryl iodides were attained with comparable regioselectivity when ferric nitrate nonahydrate was used as the catalyst with molecular iodine under 1 MPa of CO2.

机译：为铁（III）催化的有氧氧化碘化而开发了环境良性的CO2/乙二醇可逆酸性系统，而无需任何常规的酸添加剂或有机溶剂。值得注意的是，当将硝酸铁酸铁无氢水合物用作二氧化碳1 MPa以下分子碘的催化剂时，将中度至高分离的产率（高达97％）具有可比的区域选择性。

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来源
《Catalysis science & technology》 |2014年第12期|4308-4312|共5页
作者
Ma Ran; Huang Cheng-Bin; Liu An-HuaLi Xue-DongHe Liang-Nian;
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作者单位

Nankai Univ, Collaborat Innovat Ctr Chem Sci & Engn Tianjin, State Key Lab, Tianjin 300071, Peoples R China;

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正文语种英语
中图分类汉语教学;
关键词
ferric nitrate nonahydrate; Dietary Iodine; ACID ADDITIVECarbon Dioxideiodinationaromaticsacidic;

机译：硝酸铁未水解;饮食碘;酸添加二氧化碳二二氧化气囊酸酸酯;

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An in situ acidic carbon dioxide/glycol system for aerobic oxidative iodination of electron-rich aromatics catalyzed by Fe(NO3)(3).9H(2)O

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