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首页> 外文期刊>Acta crystallographica.Section D. Biological crystallography >Mosaic spread characterization of microgravity-grown tetragonal lysozyme single crystals.
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Mosaic spread characterization of microgravity-grown tetragonal lysozyme single crystals.

机译:马赛克的传播特性microgravity-grown正方溶菌酶单晶体。

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摘要

Mosaic spread values for crystals grown in microgravity were measured using synchrotron radiation. Full width at half maximum (FWHM) values for diffraction line profiles in the range 10-20" (arc seconds, 1" = 1 degrees /3600) were observed. These values are similar to those measured for crystals grown on earth using the gel-acupuncture method. The crystals analysed are composed of from two to five domains producing peaks having widths from 5 to 15". The distribution of these domains is neither homogeneous (with domains of lower quality concentrated in the centre of the crystal) nor isotropic (producing peaks whose width changes depending on the observation direction). Methodological aspects are also discussed, with special consideration of the effects of mosaic spread on the data-collection procedures for high-resolution (low-intensity) reflections.
机译:晶体生长在镶嵌分布值使用同步加速器微重力测量辐射。衍射线概要的范围值10 - 20”(弧秒,1”= 1度/ 3600)观察到。测量了晶体生长在地球上使用gel-acupuncture方法。从2到5域组成的生产山峰从5到15宽度”。这些域的分布既不是均匀(低质量的域也集中在晶体的中心)各向同性(生产峰值的宽度变化根据观察方向)。方法方面进行了讨论,特殊考虑的马赛克的影响数据收集过程的传播高分辨率反射(低强度)。

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