One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzodimidazole-5-carboxylic Acid

Mingxia Zhao; Liqin Xiong; Shilei LiJin ChangHongyu NingChuanmin Qi

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One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzodimidazole-5-carboxylic Acid

机译：封装在锌（II）、锰（II）或镍（II）原子与3-（羧甲基）-2,7-二甲基-3H-苯并咪唑-5-羧酸构成的超分子网络中的一维通道

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Four complexes with supramolecular architectures, namely, MZCA·3H_2O (1), Zn(H_2O)_6~(2+)·MZCA2·H_2O_6 (2), Mn(MZCA)_2(H_2O)_4·2H_2O (3), and Ni(MZCA)_2(H_2O)_4·2H_2O (4) MZCA = 3-(carboxymethyl)-2,7-dimethyl-3H-benzodimidazole-5-carboxylic acid, were synthesized and characterized by elemental analysis, IR spectroscopy, and single-crystal X-ray diffraction. Complexes 1 and 2 display a remarkable 3D network with 1D hydrophilic channels. Complexes 3 and 4 are isostructural and exhibit a 3D structure encapsulating 1D 24-membered ring microporous channels. The UV/Vis and fluorescent spectra were measured to characterize complexes 1-4. The thermal stability of complexes 2-4 were also examined.

机译：四种具有超分子结构的配合物，即MZCA·3H_2O（1）、[Zn（H_2O）_6]~（2+）·[MZCA]2·[H_2O]_6 （2）、[Mn（MZCA）_2（H_2O）_4]·2H_2O （3）和[Ni（MZCA）_2（H_2O）_4]·2H_2O （4） [MZCA=3-（羧甲基）-2,7-二甲基-3H-苯并咪唑-5-羧酸]，采用元素分析、红外光谱和单晶X射线衍射等手段进行了表征。配合物 1 和 2 显示出具有 1D 亲水通道的显着 3D 网络。配合物 3 和 4 是同构结构，并表现出封装 1D 24 元环形微孔通道的 3D 结构。测量紫外/可见光和荧光光谱以表征配合物 1-4。还检查了配合物2-4的热稳定性。

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来源
《Zeitschrift fur Anorganische und Allgemeine Chemie》 |2014年第1期|159-167|共9页
作者
Mingxia Zhao; Liqin Xiong; Shilei LiJin ChangHongyu NingChuanmin Qi;
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作者单位

Key Laboratory of Radiopharmaceuticals Ministry of Education, College of Chemistry Beijing Normal University Beijing, 100875, P. R. China;

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原文格式 PDF
正文语种英语
中图分类化学;
关键词
Hydrogen bonding; Channels; Water chains; X-ray diffraction; Fluorescence;

机译：氢键;频道;水链;X射线衍射;荧光;

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机译：Synthesis and Characterization of Nickel (II), Cobalt (II), Copper(II), Manganese (II), Zinc (II), Zirconium (IV), Oxomolybdenum (V), and Dioxouranium (VI) Complexes of the Schiff Base Derived from Salycylaldehyde and Thiophene-2-Carboxylic Acid Hydrazide
2. Complexes of Manganese(II), Iron(II), Cobalt(II), Nickel(II), Copper(II), and Zinc(II) with a Bishydrazone [J] . K.Mohanan, B.Murukan Synthesis and reactivity in inorganic, metal-organic, and nano-metal chemistry . 2005,第10期

机译：Complexes of Manganese(II), Iron(II), Cobalt(II), Nickel(II), Copper(II), and Zinc(II) with a Bishydrazone
3. Preparation and Spectroscopic Properties of Manganese(II), Chloroiron(III), Cobalt(II), Nickel(II), Copper(II), Zinc(II), and Cadmium(II) Complexes with Hemiporphyrazine [J] . Kazunori Sakata, Kenji Gondo, Yu-ichi HayashiMamoru Hashimoto Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry . 1991,第1期

机译：Preparation and Spectroscopic Properties of Manganese(II), Chloroiron(III), Cobalt(II), Nickel(II), Copper(II), Zinc(II), and Cadmium(II) Complexes with Hemiporphyrazine
4. catena-Polybis(3-hydroxyadamantane-1-carboxylato-κO 1)(3-hydroxyadamantane-1-carboxylic acid-κO 1)zinc(II)-μ2-44′-bipyridine monohydrate [O] . Jin-Bei Shen, Quan-Yin Guan, Xiao-Ju Chen, 2011

机译：阳离子多聚双（3-羟基金刚烷-1-羧基-κO 1）（3-羟基金刚烷-1-碳氧基酸-κO 1）zinc（II）-μ2-44-bipyridine一水合物
5. Association Involving Optically Active Ions. III. Pfeiffer Effect in Tris(phenanthroline)-zinc(II) or –nickel(II) –Alkaloid Systems [O] . Kazuko Ogino, Tokue Kumagai 1974

机译：涉及光学活性离子的关联。 III。 Tris（菲咯啉）-zinc（ii）或-Nickel（II）-alkaloid系统中的效果

One-Dimensional Channels Encapsulated in Supramolecular Networks Constructed of Zinc(II), Manganese(II), or Nickel(II) Atoms with 3-(Carboxymethyl)-2,7-dimethyl-3H-benzodimidazole-5-carboxylic Acid

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