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Multigram Scale Synthesis of Piperarborenines C-E

机译：Multigram Scale Synthesis of Piperarborenines C-E

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摘要

We report the multigram scale synthesis of heterodimeric fi-truxinic imides piperarborenines C-E using a catecholtethered diastereoselective intramolecular [2 + 2] photocycloaddition. Key innovations lie in the use of catechol as a practical auxiliary for the synthesis of homo- and heterodimeric fi-truxinates and the use of a UV-LED flow photoreactor in the [2 + 2] step. This approach is highly scalable, requiring a single column purification, no photocatalysts, and no cryogenic conditions.

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