AbstractIn this article, we demonstrate that three‐dimensional voltammetry can be used very efficiently as a reversal technique in complicated reactions. Three‐dimensional voltammetry, based on double potential step chronoamperometric data, has been used to obtain information on the reaction products of the electrochemical reduction of 4‐nitroquinoline‐N‐oxide. The study was carried out in aqueous 0.5 M HClO4solutions on Pt/Bi (upd)
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