Operando reaction cell for high energy surface sensitive x-ray diffraction and reflectometry

R. Gleissner; E. E. Beck; Simon ChungG. D. L. SemioneN. MukharamovaG. GizerC. PistiddaD. RennerH. NoeiV. VonkA. Stierle

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Operando reaction cell for high energy surface sensitive x-ray diffraction and reflectometry

机译：Operando reaction cell for high energy surface sensitive x-ray diffraction and reflectometry

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A proof of concept is shown for the design of a high pressure heterogeneous catalysis reaction cell suitable for surface sensitive x-ray diffraction and x-ray reflectometry over planar samples using high energy synchrotron radiation in combination with mass spectrometry. This design enables measurements in a pressure range from several tens to hundreds of bars for surface investigations under realistic industrial conditions in heterogeneous catalysis or gaseous corrosion studies.

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《Review of Scientific Instruments》 |2022年第7期|073902-1-073902-6|共6页
作者
R. Gleissner; E. E. Beck; Simon ChungG. D. L. SemioneN. MukharamovaG. GizerC. PistiddaD. RennerH. NoeiV. VonkA. Stierle;
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Centre for X-ray and Nano Science CXNS, Deutsches Elektronen-Synchrotron DESY, Notkestrasse 85, 22607 Hamburg, Germany;

MAPEX Core Facility for Materials Analytics, MAPEX Center for Materials and Processes, University of Bremen, 28334 Bremen, Germany;

Institute of Hydrogen Technology, Materials Technology, Helmholtz-Zentrum hereon GmbH, Max-Planck-Strasse 1, 21502 Geesthacht, Germany;

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Operando reaction cell for high energy surface sensitive x-ray diffraction and reflectometry

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