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High vinyl polybutadiene rubber/polypropylene thermoplastic elastomer blends: Optimization of internal mixing process parameters and screening of processing methods

机译:High vinyl polybutadiene rubber/polypropylene thermoplastic elastomer blends: Optimization of internal mixing process parameters and screening of processing methods

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摘要

Thermoplastic vulcanizates (TPV) composed of high vinyl polybutadiene rubber (HVPB) and polypropylene (PP) have good thermal stability and damping properties. This work aims to apply a design of experiments (Taguchi L9 orthogonal array) to optimize the mixing parameters (rotor speed, temperature, and time) for the HVPB/PP TPV. The effects of these mixing parameters on its physical and mechanical properties of HVPB/PP TPV follow the order: rotor speed > temperature and time. In the case of the master batch process, the optimum mixing parameters are 60 rpm, 180? and 8 min. Subsequently, four processes (master batch, static vulcanization, rubber-plastic premixing, and two-step processing) are compared using the same optimum mixing parameters. The master batch process turns out to be the best in terms of physical and mechanical properties.
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