Synthesis and Crystal and Molecular Structure of the Solvated Complex MoO2(L) center dot C5H5N, WhereL(2-)Is the 2-N-(2-Hydroxynaphthalidene)aminopropane-1,2,3-Triol Anion

Sergienko V. S.; Abramenko V. L.; Surazhskaya M. D.

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Synthesis and Crystal and Molecular Structure of the Solvated Complex MoO2(L) center dot C5H5N, WhereL(2-)Is the 2-N-(2-Hydroxynaphthalidene)aminopropane-1,2,3-Triol Anion

机译：Synthesis and Crystal and Molecular Structure of the Solvated Complex MoO2(L) center dot C5H5N, WhereL(2-)Is the 2-N-(2-Hydroxynaphthalidene)aminopropane-1,2,3-Triol Anion

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A new dioxomolybdenum(VI) compound MoO2(L) center dot C5H5N, whereL(2-)is 2-N-(2-hydroxynaphthalidene)aminopropane-1,2,3-triol, was synthesized and its structure was determined by IR spectroscopy and X-ray diffraction. The Mo atom is in an octahedral coordination environment formed by two oxo ligands incispositions to each other, two O atoms and the N(2) atom of the tridentate bis(chelate) ligandL, and the N(1) atom of the pyridine (Py) molecule. The N(2)(L) and N(1)(Py) atoms are intranspositions to the O(oxo) ligands at distances that are elongated due to the structuraltranseffect of the multiply bonded oxo ligands (Mo-N(1), 2.476 angstrom; Mo-N(2), 2.272 angstrom).

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《Crystallography reports》 |2020年第4期|582-585|共4页
作者
Sergienko V. S.; Abramenko V. L.; Surazhskaya M. D.;
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Russian Acad Sci, Kurnakov Inst Gen & Inorgan Chem, Moscow 119991, Russia;

Luhansk Taras Shevchenko Natl Univ, UA-92700 Lugansk, Ukraine;

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中图分类晶体学;
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Synthesis and Crystal and Molecular Structure of the Solvated Complex MoO2(L) center dot C5H5N, WhereL(2-)Is the 2-N-(2-Hydroxynaphthalidene)aminopropane-1,2,3-Triol Anion

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