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>Effect of accelerating potential on the determination of structural parameters of cellulose by electron diffraction technique
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Effect of accelerating potential on the determination of structural parameters of cellulose by electron diffraction technique
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机译：Effect of accelerating potential on the determination of structural parameters of cellulose by electron diffraction technique
AbstractAn accelerating potential of 75 kV combined with very low beam current and exposure time of 5 sec seem ideal for recording electron diffraction pattern of cooled specimens of cellulose microfibrils. Over 16 reflections could be seen distinctly. The structural parameters of ordered regions were: 89 crystallinity index, 72 Å crystallite width, and 209–230 Å crystallite length. Even the diffraction pattern of the uncooled specimen at 75 kV had a large number of reflections and was superior to those recorded on the cooled specimen at 50 or 100
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