PREPARATION AND REACTIONS OF SODIUM TELLURIDE, NA2TE - CRYSTAL STRUCTURE OF NA(CH3OH)(3)2TE2 German

Thiele KH.; Dumichen U.; Neumuller B.Steinicke A.

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PREPARATION AND REACTIONS OF SODIUM TELLURIDE, NA2TE - CRYSTAL STRUCTURE OF NA(CH3OH)(3)2TE2 German

机译：碲化钠NA的制备和反应2TE - NA（CH3OH）（3）2TE2的晶体结构德语

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Sodium telluride, Na2Te 1, is easily obtained by reaction of sodium with hexagonal tellurium in 1,2-dimethoxy-ethane in the presence of catalytic amounts of naphthalene. Upon exposure to oxygen 1 reacts with methanol forming Na(CH3OH)(3)Te-2(2) 2, which crystal structure was determined. Compound 1, prepared in situ, can be conveniently converted into dialkyl tellurides, R(2)Te (R = C2H5, i-C3H7, CH2 = CH-CH2 3). References: 32

机译：碲化钠 Na2Te 1 很容易通过钠与六方碲在 1,2-二甲氧基乙烷中的催化量萘存在下反应而获得。暴露于氧气后，1与甲醇反应生成[Na（CH3OH）（3）]Te-2（2）2，其晶体结构被确定。原位制备的化合物1可以方便地转化为二烷基碲化物R（2）Te（R=C2H5，i-C3H7，CH2=CH-CH2 3）。[参考文献： 32]

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |1996年第2期|231-234|共4页
作者
Thiele KH.; Dumichen U.; Neumuller B.Steinicke A.;
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作者单位

UNIV HALLE INST ANORGAN CHEM GEUSAER STR D-06217 MERSEBURG GERMANY;

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正文语种德语
中图分类化学;
关键词
Sodium tellurides; Dialkyl tellurides; X-ray structure; Cyclomer complexes; 1; 4; 7; 10-tetraoxacyclododecane; Selenium;

机译：碲化钠;二烷基碲化物;X射线结构;旋风复合体;1;4;7;10-四氧杂环十二烷;硒;

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1. ChemInform Abstract: Preparation and Reactions of Sodium Telluride, Na2Te ‐ Crystal Structure of (Na(CH3OH)3)2Te2. [J] . K.‐H. THIELE, A. STEINICKE, U. DUEMICHENB. NEUMUELLER Chem Inform . 1996,第20期

机译：ChemInform Abstract: Preparation and Reactions of Sodium Telluride, Na2Te ‐ Crystal Structure of (Na(CH3OH)3)2Te2.
2. ChemInform Abstract: Organic Reactions Using Sodium Hydrogen Telluride. Part 3. The Reaction of Sodium Hydrogen Telluride with α,β‐Unsaturated Carbonyl Compounds. [J] . M. YAMASHITA, Y. TANAKA, A. ARITAM. NISHIDA Chem Inform . 1994,第51期

机译：ChemInform Abstract: Organic Reactions Using Sodium Hydrogen Telluride. Part 3. The Reaction of Sodium Hydrogen Telluride with α,β‐Unsaturated Carbonyl Compounds.
3. Structure change via partial Se/Te substitution: Crystal structure and physical properties of the telluride Ba_2Cu_(4-x)Te _5in contrast to the selenide-telluride Ba_2Cu _(4-x)Se_yTe_(5-y) [J] . Mayasree O., Cui Y., Assoud A.Kleinke H. Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics . 2010,第14期

机译：Structure change via partial Se/Te substitution: Crystal structure and physical properties of the telluride Ba_2Cu_(4-x)Te _5in contrast to the selenide-telluride Ba_2Cu _(4-x)Se_yTe_(5-y)
4. Preparation and Crystal Structure of Diaqua(μ-5,5'-bistetrazolato-κ4N1,N2,N5,N6)copper(II) [O] . Manuel Joas, Thomas M. Klapötke, Jörg Stierstorfer 2012

机译：preparation and Crystal structure of Diaqua(μ-5,5'-bistetrazolato-κ4N1,N2,N5,N6)copper(II)

PREPARATION AND REACTIONS OF SODIUM TELLURIDE, NA2TE - CRYSTAL STRUCTURE OF NA(CH3OH)(3)2TE2 German

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