SYNTHESIS AND PROPERTIES OF N,N-DIALKYL-ALLYLAMINOBORANES AND N,N-DIMETHYLAMINOPROPYLBORANE German

Thiele KH.; Dumichen U.; Kurzhals R.

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SYNTHESIS AND PROPERTIES OF N,N-DIALKYL-ALLYLAMINOBORANES AND N,N-DIMETHYLAMINOPROPYLBORANE German

机译：N，N-二烷基-烯丙基氨基硼烷和N，N-二甲氨基丙基硼烷的合成与性能德语

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Complexes of the type H3B<--NR(2)(CH2CH=CH2) (R=CH3 I, C2H5 II) are formed by reaction of LiBH4 with dialkylallylammonium salts. By addition of AlCl3 I can be transformed into the chelate-stabilized N,N-dimethyl-amino-propylborane H2B-CH2-CH2-CH2-NMe(2) III. The i.r.-, H-1, C-13-n.m.r. and mass-spectra of I - III are reported and discussed. References: 10

机译：H3B<--NR（2）（CH2CH=CH2）（R=CH3 I， C2H5 II）型络合物由Li[BH4]与二烷基烯丙基铵盐反应形成。通过添加 AlCl3 I，可以转化为螯合物稳定的 N，N-二甲基氨基丙基硼烷 H2B-CH2-CH2-CH2-NMe（2） III。报道并讨论了I-III的i.r.-、H-1、C-13-n.m.r.和质谱。[参考文献： 10]

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《Zeitschrift fur Anorganische und Allgemeine Chemie》 |1995年第1期|97-100|共4页
作者
Thiele KH.; Dumichen U.; Kurzhals R.;
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作者单位

MARTIN LUTHER UNIV HALLE WITTENBERG INST ANORGAN CHEM GEUSAER STR 88 D-06217 MERSEBURG GERMANY;

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正文语种德语
中图分类化学;
关键词
Boranes; Borazanes; Organoboron chelate compounds; Nmr spectra;

机译：硼烷;硼烷;有机硼螯合物;核磁共振波谱;

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SYNTHESIS AND PROPERTIES OF N,N-DIALKYL-ALLYLAMINOBORANES AND N,N-DIMETHYLAMINOPROPYLBORANE German

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