Cryogenic implementation of charging diamond anvil cells with H_(2) and D_(2)

Zhenhua Chi; Huyen Nguyen; Takahiro MatsuokaTomoko KagayamaNaohisa HiraoYasuo OhishiKatsuya Shimizu

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Cryogenic implementation of charging diamond anvil cells with H_(2) and D_(2)

机译：Cryogenic implementation of charging diamond anvil cells with H_(2) and D_(2)

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摘要

A cryogenic loading system for introducing H_(2) and D_(2) into the diamond anvil cell has been designed and constructed. The integration of pressure loading mechanism, ruby fluorescence spectrometer, and microscope camera allows for in situ tuning and calibrating the pressure. The performance of the system has been demonstrated by successful synthesis of hydride and deuteride of transition metal and rare earth metal. Our cryogenic methodology features facile start-over of loading and in situ electrical resistance measurement of as-synthesized sample.

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来源
《Review of Scientific Instruments》 |2011年第10期|105109-1-105109-4|共4页
作者
Zhenhua Chi; Huyen Nguyen; Takahiro MatsuokaTomoko KagayamaNaohisa HiraoYasuo OhishiKatsuya Shimizu;
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KYOKUGEN, Center for Quantum Science and Technology under Extreme Conditions, Osaka University, Osaka 560-8531, Japan;

Japan Synchrotron Radiation Research Institute (JASRI)/SPring-8, Hyogo 679-5198, Japan;

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正文语种英语
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Cryogenic implementation of charging diamond anvil cells with H_(2) and D_(2)

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