Solid-state compounds of 2-chlorobenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behaviour

Bannach  G; Siqueira  AB; Ionashiro  EYRodrigues  ECIonashiro  M

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Solid-state compounds of 2-chlorobenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behaviour

机译：2-氯亚苄基丙酮酸与一些二价金属离子的固态化合物 - 合成、表征和热行为

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摘要

Solid-state M-2-Cl-BP, where M stands for Mn, Fe, Co, Ni, Cu, Zn and Pb and 2-Cl-BP is 2-chlorobenzylidenepyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), simultaneous thermogravimetry and differential thermal analysis (TG-DTA), X-ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated compounds.

机译：已经合成了固态 M-2-Cl-BP，其中 M 代表 Mn、Fe、Co、Ni、Cu、Zn 和 Pb，2-Cl-BP 代表 2-氯亚苄基丙酮酸。采用热重法和衍生热重法（TG/DTG）、同步热重法和差热分析法（TG-DTA）、X射线粉末衍射法、红外光谱法、元素分析法和络合法来表征和研究这些化合物的热行为。结果导致了有关分离化合物的组成、脱水、热稳定性和热分解的信息。

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来源
《Journal of thermal analysis and calorimetry》 |2007年第3期|873-879|共7页
作者
Bannach G; Siqueira AB; Ionashiro EYRodrigues ECIonashiro M;
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作者单位

UNESP, Inst Quim, BR-14801970 Araraquara, SP, Brazil;

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原文格式 PDF
正文语种英语
中图分类分析化学;
关键词
bivalent metals; 2-chlorobenzylidenepyruvate; coordination sites; thermal behaviour; LIGHTER TRIVALENT LANTHANIDES; ACIDS;

机译：二价金属;2-氯亚苄基丙酮酸酯;协调站点;热性能;打火机 TRIVALENT LANTHANIDES;酸;

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Solid-state compounds of 2-chlorobenzylidenepyruvate with some bivalent metal ions - Synthesis, characterization and thermal behaviour

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