Synthesis and Crystal Structure of a Novel Mn(II) Coordination Polymer with 3-(4-(1H-Benzodimidazol-1-yl)-4-methoxyphenyl)-1-phenylprop-2-en-1-one Ligands

Wang G. -F.; Zhang X.; Sun S. -W.Han Q. -P.Yang X.Li H.Ma H. -X.Yao C. -Z.Sun H.Dong H. -B.

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Synthesis and Crystal Structure of a Novel Mn(II) Coordination Polymer with 3-(4-(1H-Benzodimidazol-1-yl)-4-methoxyphenyl)-1-phenylprop-2-en-1-one Ligands

机译：3-（4-（1H-苯并咪唑-1-基）-4-甲氧基苯基）-1-苯基丙-2-烯-1-酮配体的新型Mn（II）配位聚合物的合成及晶体结构

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3-(4-(1H-Benzodimidazol-1-yl)-4-methoxyphenyl)-1-phenylprop-2-en-1-one (L-1 , 1) and its Mn(II) complex, Mn(L-1 )(2)(SCN)(2)(infinity) (2), were synthesized and characterized by elemental analyses, IR spectroscopy and single-crystal X-ray diffraction. The Mn(II) ion in 2 is six-coordinated to four nitrogen atoms of two L-1 ligands, two SCN-ligands, and two oxygen atoms of other two L (1) ligands to form a distorted octahedral geometry. Therefore, each L-1 links Mn ions through the O and N atoms to generate 2D sheet structure.

机译：通过元素分析、红外光谱和单晶X射线衍射等手段合成了3-（4-（1H-苯并[d]咪唑-1-基）-4-甲氧基苯基）-1-苯基丙-2-烯-1-酮（L-1,1）及其Mn（II）配合物[Mn（L-1 ）（2）（SCN）（2）]（无穷大）（2）。2 中的 Mn（II）离子与两个 L-1 配体、两个 SCN 配体的四个氮原子和其他两个 L （1）配体的两个氧原子六配位，形成扭曲的八面体几何形状。因此，每个 L-1 通过 O 和 N 原子连接 Mn 离子以产生 2D 片状结构。

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来源
《Crystallography reports》 |2015年第7期|1038-1043|共6页
作者
Wang G. -F.; Zhang X.; Sun S. -W.Han Q. -P.Yang X.Li H.Ma H. -X.Yao C. -Z.Sun H.Dong H. -B.;
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Yuncheng Univ, Dept Appl Chem, Yuncheng 044000, Peoples R China;

Harbin Inst Technol, Acad Fundamental & Interdisciplinary Sci, Harbin 150080, Heilongjiang, Peoples R China;

Jilin Med Coll, Coll Pharm, Zhengzhou 132013, Jilin, Peoples R China;

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Synthesis and Crystal Structure of a Novel Mn(II) Coordination Polymer with 3-(4-(1H-Benzodimidazol-1-yl)-4-methoxyphenyl)-1-phenylprop-2-en-1-one Ligands

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