Synthesis, Characterization, and Crystal Structure of 2-Amino-5-oxo-4-phenyl-4,5-dihydropyrano3,2-cchromene-3-carbonitrile

Sharma S.; Brahmachari G.; Banerjee B.Kant R.Gupta V. K.

首页> 外文期刊>Crystallography reports >Synthesis, Characterization, and Crystal Structure of 2-Amino-5-oxo-4-phenyl-4,5-dihydropyrano3,2-cchromene-3-carbonitrile

【24h】

Synthesis, Characterization, and Crystal Structure of 2-Amino-5-oxo-4-phenyl-4,5-dihydropyrano3,2-cchromene-3-carbonitrile

机译：2-氨基-5-氧代-4-苯基-4,5-二氢吡喃并3,2-c苯并吡喃-3-甲腈的合成、表征及晶体结构

获取原文

获取原文并翻译 | 示例

掌桥外文数据库（机构版） >>

开具论文收录证明 >>

文献代查 >>

页面导航

摘要
著录项
相似文献
相关主题

摘要

The title compound, 2-amino-5-oxo-4-phenyl-4,5-dihydropyrano3,2-cchromene-3-carbonitrile was synthesized in excellent yield by one-pot multicomponent reaction and its crystal structure is determined by X-ray structure analysis. The crystals are monoclinic, sp. gr. P2(1)/c, a = 9.0750(6), b = 13.2729(8), c = 12.6892(9) angstrom, beta = 96.975(6)degrees, Z = 4; R = 0.0466 for 1771 observed reflections. The crystal structure is stabilized by N-H center dot center dot center dot N, N-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds. In addition, C-H center dot center dot center dot pi and pi center dot center dot center dot pi interactions are observed in the crystal structure.

机译：采用一锅法多组分反应合成了2-氨基-5-氧代-4-苯基-4,5-二氢吡喃并[3,2-c]苯并吡喃-3-甲腈，收率优异，X射线结构分析测定了其晶体结构。晶体是单斜晶系，sp. gr。P2（1）/c，a = 9.0750（6），b = 13.2729（8），c = 12.6892（9）埃，β = 96.975（6）度，Z = 4;R = 0.0466 表示 1771 次观测反射。晶体结构由N-H中心点中心点N、N-H中心点中心点、中心点O和C-H中心点中心点点O氢键稳定。此外，在晶体结构中还观察到 C-H 中心点中心点中心点 pi 和 pi 中心点中心点中心点 pi 相互作用。

著录项

来源
《Crystallography reports》 |2015年第7期|1142-1146|共5页
作者
Sharma S.; Brahmachari G.; Banerjee B.Kant R.Gupta V. K.;
展开▼
作者单位

Univ Jammu, Postgrad Dept Phys Elect, Xray Crystallog Lab, Jammu 180006, India;

Visva Bharati, Dept Chem, Lab Nat Prod & Organ Synth, Santini Ketan 731235, W Bengal, India;

展开▼
收录信息
原文格式 PDF
正文语种英语
中图分类晶体学;
关键词

相似文献

外文文献
中文文献
专利

1. Synthesis,X-ray crystal structure,Hirshfeld surface analysis,and molecular docking studies of DMSO/H2O solvate of 5-chlorospiroindoline-3,7'-pyrano3,2-c:5,6-c'dichromene-2,6',8'-trione [J] . Varun Sharma, Bubun Banerjee, Aditi Sharma European Journal of Chemistry . 2021,第4期

机译：Synthesis,X-ray crystal structure,Hirshfeld surface analysis,and molecular docking studies of DMSO/H2O solvate of 5-chlorospiroindoline-3,7'-pyrano3,2-c:5,6-c'dichromene-2,6',8'-trione
2. SYNTHESIS AND X-RAY CRYSTAL STRUCTURE OF (μ-H)_2(Cl)Os_3(CO)_8{μ_3-η~2-C(C_9H_5)(4-CH_3)N} [J] . IQBAL HYDER, SHARIFF E. KABIR, ARZU MIAHABDUL MOTTALIBK. M. ABDUL MALIK Journal of the Bangladesh Academy of Sciences . 2003,第2期

机译：SYNTHESIS AND X-RAY CRYSTAL STRUCTURE OF (μ-H)_2(Cl)Os_3(CO)_8{μ_3-η~2-C(C_9H_5)(4-CH_3)N}
3. Synthesis, crystal structure, spectral characterization and Hirshfeld surface analysis of (E)-N ' -(3-ethoxy-4-hydroxybenzylidene)-4-fluorobenzohydrazide single-crystal-a novel NLO active material [J] . Shobana D., Sudha S., Ramarajan D.Dimic D. Journal of Molecular Structure . 2022,第2期

机译：Synthesis, crystal structure, spectral characterization and Hirshfeld surface analysis of (E)-N ' -(3-ethoxy-4-hydroxybenzylidene)-4-fluorobenzohydrazide single-crystal-a novel NLO active material
4. Synthesis and Characterization of YAG:Ce Phosphor by Microwave Induced Combustion Synthesis with Different Fuel Sources [C] . Khai Shenn Lau, Zainuriah Hassan, Way Foong Lim, International Conference on Semiconductor Materials and Technology . 2019

机译：Synthesis and Characterization of YAG:Ce Phosphor by Microwave Induced Combustion Synthesis with Different Fuel Sources
5. Do crystal structures obviate the need for theoretical models of GPCRs for structure based virtual screening [O] . Hao Tang, Xiang Simon Wang, Jui-Hua Hsieh, -1

机译：Crystal Structures是否需要基于结构的虚拟筛选的GPCR理论模型
6. Hydrothermal synthesis and characterization of microporous crystals of trivalent metal-containing zirconium phosphates [O] . Sun ZG, Liu ZM, Xu L, 2004

机译：Hydrothermal synthesis and characterization of microporous crystals of trivalent metal-containing zirconium phosphates
7. Synthesis and Characterization of z-N3NFO+ and e-N3NFO+ (Postprint) [R] . Wilson, W. W., Haiges, R., Christie, K. O., 2007

机译：synthesis and Characterization of z-N3NFO+ and e-N3NFO+ (postprint)

Synthesis, Characterization, and Crystal Structure of 2-Amino-5-oxo-4-phenyl-4,5-dihydropyrano3,2-cchromene-3-carbonitrile

摘要

著录项

相似文献

相关主题

期刊订阅