Application of Cocrystallization for the Separation of C-Ethylresorcin6arene from C-Ethylresoricn4arene

Jiang Shan; Patil Rahul S.; Barnes Charles L.Atwood Jerry L.

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Application of Cocrystallization for the Separation of C-Ethylresorcin6arene from C-Ethylresoricn4arene

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Cocrystals formed from macrocyclic compounds such as calixarenes are particularly useful for understanding various host guest interactions and solid state properties. Resorcinarenes, a subclass of calixarenes, are also useful for the construction of cocrystalline materials because of their unique bowl shape, decorated with eight hydroxyl groups. Here we investigate the separation of hexameric C-ethylresoricn6arene from its tetrameric homologues C-ethylresorcin4arene via cocrystallization with 4,4'-bipyridine (Scheme 1). The effect of the stoichiometric ratio of the components and the solvent of crystallization on the separation of macrocycles and on the formation of a particular cocrystal is also discussed.

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《Crystal growth & design》 |2017年第8期|4060-4063|共4页
作者
Jiang Shan; Patil Rahul S.; Barnes Charles L.Atwood Jerry L.;
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Univ Missouri, Dept Chem, Columbia, MO 65211 USA;

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正文语种英语
中图分类晶体学;
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Application of Cocrystallization for the Separation of C-Ethylresorcin6arene from C-Ethylresoricn4arene

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