Crystal structure of tetrachlorobis #mu#-imidocarbonylchloridatodiboron

Doyle Britton; Kenneth Emerson

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Crystal structure of tetrachlorobis #mu#-imidocarbonylchloridatodiboron

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Boron trichloride and mercuric cyanide react slowly to form the title compound, B_2N_2C_2Cl_8, which contains a four-membered B_2N_2 ring with alternating BCl_2 and N = CCl_2. Crystals are triclinic, space group P1-bar, a = 6.1198(1), b = 7.4457(3), c = 7.9186(3) A, #alpha# = 117.064(2), #beta# = 106.923, #gamma# = 93.712(2) deg, Z = 1, and V = 299.07(2) A~3. The compound has a crystallographic center of symmetry but the metric symmetry is close to the expected mmm.

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《Journal of chemical crystallography》 |1999年第7期|841-844|共4页
作者
Doyle Britton; Kenneth Emerson;
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作者单位

Department of Chemistry, University of Minnesota, Minneapolis, Minnesota 55455-0431;

Department of Chemistry, Montana State University, Bozeman, Montana 59717-0340;

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正文语种英语
中图分类晶体学;
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boron-nitrogen heterocycles;

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Crystal structure of tetrachlorobis #mu#-imidocarbonylchloridatodiboron

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